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退火温度对Ti-Ni-Cr低温超弹性合金组织和拉伸性能的影响
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陕西省自然科学基金 (2009JM6010);陕西省教育厅科研计划 (09JK375)


Effects of Annealing Temperatures on Microstructure and Tensile Properties of Ti-Ni-Cr Low-Temperature Superelastic Alloy
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    摘要:

    用光学显微镜和拉伸试验研究了退火温度 (Ta) 对Ti-50.8Ni-0.3Cr合金显微组织和拉伸行为的影响。结果表明,合金原始态为拉拔纤维组织,退火时发生回复与再结晶。Ta =350~500 ℃时,为回复阶段,组织呈纤维状。Ta =550~590 ℃时,为再结晶阶段,纤维组织逐渐变成无畸变等轴晶粒,再结晶温度在570 ℃左右。Ta =600~800 ℃时,为晶粒长大阶段,显微组织呈粗大不均匀等轴晶。Ta对合金在低温 (8 ℃)下的拉伸行为有显著影响,随Ta升高,应力诱发马氏体相变临界应力先降低后升高;350~500 ℃退火态合金的加工硬化能力和抗拉强度大于550~700 ℃退火态合金,而后者的延伸率则显著大于前者。当Ta大于650 ℃后合金的延伸率因晶粒粗化而减小

    Abstract:

    effects of annealing temperatures (Ta) on microstructure and tensile behavior of Ti-50.8Ni-0.3Cr (at%) low-temperature superelastic alloy were investigated by optical microscopy and tensile tests. The results show that, the microstructure of the as-received alloy is fibriform, and the recovery and the recrystallization occur in the alloy during annealing. When Ta =350-500 oC, the alloy is at the recovery stage, and the microstructure is fibriform. When Ta =550-590 oC, the alloy is at the recrystallization stage, the microstructure turns to the unstrained equiaxed grains, and the recrystallization temperature of the alloy is about 570 oC. when Ta =600-800 oC, the alloy is at the grain growth stage, the microstructure shows larger and asymmetrical grains. Ta also strongly influences the tensile behavior of the alloy at low temperature (8 oC). With increasing of Ta, the critical stress of the stress-induced martensitic transformation declines at first and then rises; the work hardening ability and the tensile strength of the alloy annealed at 350-500 oC are higher than those of the alloy annealed at 550-700 oC, but the elongation of the latter is significantly larger than that of the former. When Ta >650 oC, the elongation of the alloy decreases due to the grain growth.

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贺志荣,王 启,王 芳,王永善,杨 军.退火温度对Ti-Ni-Cr低温超弹性合金组织和拉伸性能的影响[J].稀有金属材料与工程,2011,40(11):1998~2001.[He Zhirong, Wang Qi, Wang Fang, Wang Yongshan, Yang Jun. Effects of Annealing Temperatures on Microstructure and Tensile Properties of Ti-Ni-Cr Low-Temperature Superelastic Alloy[J]. Rare Metal Materials and Engineering,2011,40(11):1998~2001.]
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  • 收稿日期:2010-11-23
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