+高级检索
Effects of C10H8 Doping on Microstructure and Superconductivity of MgB2 Wires
DOI:
作者:
作者单位:

作者简介:

通讯作者:

中图分类号:

基金项目:


Effects of C10H8 Doping on Microstructure and Superconductivity of MgB2 Wires
Author:
Affiliation:

Fund Project:

“863” Project (2007AA03Z237),the National Key Basic Research Program (No. 2011CBA00104) of China

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    采用原位粉末装管技术(in-situ PIT)制备了萘(C10H8)掺杂MgB2/Nb/Cu线材。前驱粉末按照MgB2+xwt% (x=0,2,5,8)的比例将Mg粉、B粉和C10H8粉末混合研磨,装入Cu/Nb复合管中,分别拉拔加工至Φ2.0 mm和Φ1.0 mm,然后Ar气氛中分别在650,700,750 ℃热处理,保温2.5 h。通过X射线衍射仪(XRD)、扫描电子显微镜(SEM)和能谱仪(EDS)等测试手段分析了样品的相结构和微观结构等。结果发现,样品超导转变温度Tc不随萘掺杂量的变化而变化,但正常态电阻有所降低。在20和25 K无外磁场时,x=8样品的临界电流密度分别达到1.1×105和3.8×104 A/cm2,而x=5样品也达到3.1×104 和 1.2×104 A/cm2。

    Abstract:

    C10H8-doped MgB2 wires were fabricated by in-situ PIT (Powder in Tube) method. The Nb/Cu tube was filled with the uniformly mixed precursor powders of magnesium, boron and C10H8 with the stoichiometry of MgB2+xwt%C10H8 ,where x=0, 2, 5, 8 and drawn to diameter Φ2 mm and Φ1 mm, respectively, and then heat treated in argon atmosphere at three different temperatures (650, 700, 750 ℃) for 2.5 h. The phase formation and microstructures of the samples were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), and so on. It is found that the critical transition temperature (Tc) changes little with increasing of C10H8 doping content, while normal resistance decreases to some degree. At 20, 25 K and in zero external field, the critical current density (Jc) the sample of x=8 achieves 1.1×105 and 3.8×104 A/cm2, respectively, and the Jc of the sample of x=5 reaches 3.1×104 and 1.2×104 A/cm2, respectively.

    参考文献
    相似文献
    引证文献
引用本文

孙昱艳,张平祥,熊晓梅,刘国庆,闫 果. Effects of C10H8 Doping on Microstructure and Superconductivity of MgB2 Wires[J].稀有金属材料与工程,2012,41(1):5~8.[Sun Yuyan, Zhang Pingxiang, Xiong Xiaomei, Liu Guoqing, Yan Guo. Effects of C10H8 Doping on Microstructure and Superconductivity of MgB2 Wires[J]. Rare Metal Materials and Engineering,2012,41(1):5~8.]
DOI:[doi]

复制
文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2011-01-11
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期:
  • 出版日期: