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等通道转角挤压变形Mg-1.5Mn-0.3Ce镁合金的组织、织构与力学性能
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广州市科技支撑计划项目(2009Z2-D811)


Microstructure, Texture and Mechanical Properties of Mg-1.5Mn-0.3Ce Magnesium Alloy Deformed by Equal Channel Angular Pressing
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    摘要:

    采用等通道转角挤压(ECAP)工艺以Bc路径在623 K温度下对Mg-1.5Mn-0.3Ce镁合金进行变形,观察显微组织与织构,测试了力学性能。显微组织分析表明,镁合金经ECAP变形晶粒尺寸明显得到细化,经6道次ECAP变形后晶粒尺寸由原轧制态的约26.1 μm细化至约1.2 μm,且细小的第二相粒子Mg12Ce弥散分布于晶内及晶界处;同时经ECAP变形后,原始轧制织构随变形道次的增加不断减小,并开始转变为ECAP织构,织构强度不断增强;力学性能结果表明,由于晶粒细化作用大于织构软化作用,前3道次ECAP变形镁合金强度随道次的增加不断提高,与Hall?Petch关系相符,在第3道次时其抗拉强度和屈服强度达到最大值,分别为272.2和263.7 MPa;在4道次之后形成较强的非基面织构,镁合金强度下降,与Hall?Petch呈相悖关系。断口分析表明,轧制态与ECAP变形镁合金的断裂方式都是沿晶断裂,由于6道次变形镁合金晶粒细化,存在更多的韧窝并获得16.8 %最大室温伸长率。

    Abstract:

    Equal-channel angular pressing (ECAP) was conducted on Mg-1.5Mn-0.3Ce magnesium alloy at 623 K using route Bc to investigate its microstructure, the texture and mechanical properties. The microstructure observation indicates that grains are obviously refined by ECAP, the smallest grain size of ECAPed magnesium alloy is about 1.2 μm after sixth pass ECAP from 26.1 μm of as-rolled one, and numbers of tiny Mg12Ce dispersively distribute in intragranular and intergranular regions. At the same time, the texture of as-rolled magnesium alloy is reduced gradually and starts to change to ECAPed texture when the texture intensity rises with the increase of ECAP passes. Mechanical properties show that the tensile strength and yield strength are raised with ECAP passes before three passes, matching the relationship of Hall-Petch because grain refinement is more significant than texture softening, and gets the maximum values of 272.2 MPa and 263.7 MPa at the third pass deformation. When the passes continue to increase to four passes, the strength is declined in contradiction to Hall-Petch relationship due to formed non-basic texture. The tensile-to-failure morphologies reveal that fractured mode is along the grain boundary for as-rolled and ECAPed magnesium alloys, and there are more dimples for sixth pass with the biggest elongation of 16.8 % at room temperature.

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康志新,彭勇辉,孔 晶,简炜炜,李元元.等通道转角挤压变形Mg-1.5Mn-0.3Ce镁合金的组织、织构与力学性能[J].稀有金属材料与工程,2012,41(2):215~220.[Kang Zhixin, Peng Yonghui, Kong Jing, Jian Weiwei, Li Yuanyuan. Microstructure, Texture and Mechanical Properties of Mg-1.5Mn-0.3Ce Magnesium Alloy Deformed by Equal Channel Angular Pressing[J]. Rare Metal Materials and Engineering,2012,41(2):215~220.]
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  • 收稿日期:2011-02-14
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