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ECHE挤压对AZ31镁合金组织和性能的影响
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国家科技重大专项(2009ZX04005-031-11);“111”引智计划(B08040)


Effect of ECHE Forming on the Microstructure and Mechanical Properties of AZ31 Magnesium Alloy
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    摘要:

    提出了等通道螺旋转角挤压(equal channel helix angular extrusion,ECHE)变形方法,采用Deform-3D平台的有限元模拟、OM、SEM、TEM、拉伸试验等方法,研究了ECHE 制造AZ31镁合金轻质螺栓坯料的挤压工艺、温度场、合金流动情况、组织和性能。结果表明:在变形温度为380 ℃,挤压速度为3 mm·s-1时,合金变形均匀,不易出现挤压缺陷;等通道螺旋转角挤压变形可以显著细化AZ31镁合金晶粒;其挤压过程中晶粒细化机制为晶粒破碎和动态再结晶;挤压后的平均晶粒尺寸为3~5 μm,且合金晶粒大小均匀;力学性能较铸态大幅度提高,室温抗拉强度和屈服强度分别由209和104 MPa提高到286和165 MPa,延伸率由11%提高到26.4%,拉伸断口呈现为韧窝断裂和准解理断裂的混合特征。

    Abstract:

    A deformation technique of the equal channel helix angular extrusion (ECHE) was proposed. Extrusion process, temperature field, metal flow, microstructure and mechanical properties of ECHE AZ31 magnesium alloy were investigated by Deform-3D FEM, OM, SEM, TEM and tensile experiments. The results show that metal flow is symmetrical and there is no disfigurement at the temperature of 380 oC and extrusion rate of 3 mm·s-1. The ECHE could evidently refine the grains of the alloy. The mechanism of grain refinement is grain fragmentation and dynamic recrystallization. The mean grain size after extrusion is 3~5 μm and the material is deformed homogeneously. The mechanical properties are greatly improved. The tensile strength, yield strength and elongation of the sample are increased from 209 MPa, 104 MPa and 11% to 286 MPa, 165 MPa and 26.4%, respectively. The tensile fracture combines the dimple fracture with quasi-cleavage fracture.

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石 磊,杨 合,郭良刚,党 利,张保军,郑文达,张 君. ECHE挤压对AZ31镁合金组织和性能的影响[J].稀有金属材料与工程,2012,41(11):1955~1959.[Shi Lei, Yang He, Guo Lianggang, Dang Li, Zhang Baojun, Zheng Wenda, Zhang Jun. Effect of ECHE Forming on the Microstructure and Mechanical Properties of AZ31 Magnesium Alloy[J]. Rare Metal Materials and Engineering,2012,41(11):1955~1959.]
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  • 收稿日期:2011-11-29
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