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放电等离子烧结TaC/Ti复合材料的组织与力学性能
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Microstructure and Mechanical Properties of TaC/Ti Composite Prepared by SPS
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    摘要:

    采用放电等离子烧结(SPS)制备碳化钽(TaC)颗粒增强钛基复合材料,通过X射线衍射仪、扫描电镜和电子探针分析了复合材料的微观组织和力学性能。结果表明:SPS制备方法在温度高于800 ℃烧结可得到致密TaC/Ti复合材料;TaC显著提高钛的硬度和强度,加入5%TaC复合材料的维氏硬度高于500 MPa,抗弯强度高于600 MPa;烧结过程中发生固相扩散反应,TaC与金属钛反应被消耗,析出分布均匀的(Ti,Ta)C1-x碳化物,分解出的Ta固溶于钛金属基体;第二相强化与固溶强化2种强化机制的共同作用使复合材料强度、硬度大幅度提高

    Abstract:

    Tantalum carbide (TaC) particles reinforced titanium composites were prepared by sparking plasma sintering (SPS). Microstructure and mechanical properties were analyzed by X-ray diffraction, scanning electron microscope and electron probe. The results show that densified TaC/Ti composite can be obtained when sintering above 800 ℃ by SPS. The hardness and strength of titanium can be significantly improved by adding TaC. The hardness of samples with 5%TaC addition are higher than 500 MPa and the bending strength are higher than 600 MPa. The original TaC was consumed owing to solid phase diffusion and reaction in the sintering process;. A new phase of (Ti, Ta)C1-x carbide was formed, which distributed uniformly around titanium matrix. The tantalum has been found in titanium matrix, which means solid solution is formed. The great improvement of the composite strength is associated with phase strengthening and solution strengthening mechanism

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杨西亚,郭玉忠,陈昱潼,淡露露,王剑华.放电等离子烧结TaC/Ti复合材料的组织与力学性能[J].稀有金属材料与工程,2013,42(11):2274~2278.[Yang Xiya, Guo Yuzhong, Chen Yutong, Dan Lulu, Wang Jianhua. Microstructure and Mechanical Properties of TaC/Ti Composite Prepared by SPS[J]. Rare Metal Materials and Engineering,2013,42(11):2274~2278.]
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  • 收稿日期:2012-11-05
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