+高级检索
电渣重熔连续定向凝固Rene88DT合金组织与偏析行为
DOI:
作者:
作者单位:

钢铁研究总院

作者简介:

通讯作者:

中图分类号:

基金项目:

国家自然科学基金资助(50735001,50675089,50975127)


Structure and segregation behavior of Rene88DT alloy prepared by ESR-CDS?
Author:
Affiliation:

Central Iron and Steel Research Institute

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    利用电渣重熔连续定向凝固技术(ESR-CDS)成功制备了Rene88DT高温合金铸锭。借助于金相显微镜,带有能谱的扫描电镜以及透射电镜,对电渣重熔连续定向合金Rene88DT铸锭进行分析,并与传统电渣铸锭进行了对比。研究结果显示,电渣重熔连续定向凝固合金Rene88DT铸锭消除了最为严重的中心偏析,中心偏析在传统电渣铸锭中是普遍存在的,这种偏析存在于柱状晶与等轴晶交界处或者柱状晶之间相互交界面处。此外,电渣重熔连续定向凝固合金二次枝晶间距较传统电渣铸锭小,析出相尺寸也较小。由于微观偏析程度的降低,使得合金在经过1200℃/24h后的热处理即可达到均匀化效果。夹杂物统计结果显示,电渣重熔连续定向凝固合金夹杂物最大尺寸为5.89微米,与传统电渣合金和粉末合金相比夹杂物数量降低60%。电渣重熔连续定向凝固合金宏观偏析和夹杂物水平的降低可提高热加工塑性,为铸&锻工艺实施提供基础。

    Abstract:

    Abstract:Directionally solidified Rene88DT superalloy ingots were successfully produced by electroslag remelting continuous directional solidification (ESR-CDS) technology. Compared with conventional ESR ingot, the as-cast structures of ESR-CDS Rene88DT alloy ingot were analyzed using by optical microscopy (OM)、field emission scanning electron microscopy (FESEM) with energy spectrum and transmission electron microscopy(TEM). The results showed that the ESR-CDS Rene88DT alloy ingot eliminated the region of the severe central segregation which existed commonly in the conventional ESR ingot because of the formation of intersection of interfaces between columnar crystal and equiaxed crystal or columnar crystal each other. In addition, the ESR-CDS Rene88DT alloy ingot showed smaller secondary dendritic spacing, smaller non-equilibrium precipitates phase. Due to the decreasing micro-segregation level, uniform distribution of alloy elements can be achieved when subjected to the heat treatment at 1200 oC for 24h. Statistical results of inclusions revealed that the maximum size of inclusion in the ESR-CDS Rene88DT alloy was not more than 5.89μm and the inclusion volume reduced by 60% compared with conventional ESR and P/M respectively. The hot working plasticity of directionally solidified Rene88DT superalloy can be improved, which makes a basis for implementation of cast-and-wrought (C&W) route.

    参考文献
    相似文献
    引证文献
引用本文

李福林.电渣重熔连续定向凝固Rene88DT合金组织与偏析行为[J].稀有金属材料与工程,2016,45(6):1437~1442.[lifulin. Structure and segregation behavior of Rene88DT alloy prepared by ESR-CDS?[J]. Rare Metal Materials and Engineering,2016,45(6):1437~1442.]
DOI:[doi]

复制
文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2014-04-20
  • 最后修改日期:2014-11-21
  • 录用日期:2014-12-25
  • 在线发布日期: 2016-10-08
  • 出版日期: