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超细晶反挤压Mg-8Sn-1Al-1Zn合金的组织和性能
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山西省青年科技基金 (2013021013-4);山西省留学回国人员择优资助项目 (2013-68)


Microstructure and Mechanical Properties of Indirect-Extruded Mg-8Sn-1Al-1Zn Alloy with Ultrafine Grained Structure
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    摘要:

    采用OM、SEM、XRD、EBSD、TEM和电子材料试验机等手段研究了超细晶反挤压Mg-8%Sn-1Al-1Zn(质量分数)合金的组织和力学性能。结果表明:在250 ℃下,通过反挤压可以制备出具有超细晶组织的高强度Mg-8Sn-1Al-1Zn合金。在反挤压过程中,大部分粗大晶粒均通过动态再结晶转变为细小的等轴晶,其平均晶粒尺寸为1.92 μm。另外,合金中存在大量的微米和纳米级Mg2Sn颗粒相。反挤压合金表现出典型的基面纤维织构。上述组织特征是动态再结晶、孪晶和第二相共同作用的结果。合金的室温抗拉屈服强度和压缩屈服强度分别为285 和260 MPa,合金的拉伸/压缩屈服点比率R高达0.91。合金的高强度和高R值主要归因于合金的细晶组织以及弥散分布的微纳米级第二相

    Abstract:

    The microstructure evolution and mechanical properties of indirect-extruded Mg-8Sn-1Al-1Zn have been investigated by OM, SEM, XRD, EBSD, TEM and a stand universal testing machine. The results indicate that the high strength Mg-8Sn-1Al-1Zn alloy with ultrafine grained structure can be successfully fabricated by indirect extrusion at 250 oC. During the extrusion process, most of the coarse grains were changed into fine equiaxed grains with average sizes of 1.92 μm. In addition, some nano-sized particles were observed by TEM in the alloy. The extruded alloy reveals a type of fiber texture in which basal poles are preferentially perpendicular to the ED. The formation of the ultra-fine grained structure was ascribed to the dynamic recrystallization and second phase. The tensile yield strength and compressive yield strength of the extruded alloys are 285 and 260 MPa, respectively. The R value of the alloy equals to 0.91. The superior strength and low yield asymmetry are mainly related to the fine-grained structure and dispersive fine second phase particles

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程伟丽,霍 瑞,陆杨婕,You Bong-sun, Park Sung-soo.超细晶反挤压Mg-8Sn-1Al-1Zn合金的组织和性能[J].稀有金属材料与工程,2014,43(11):2824~2828.[Cheng Weili, Huo Rui, Lu Yangjie, You Bong-sun, Park Sung-soo. Microstructure and Mechanical Properties of Indirect-Extruded Mg-8Sn-1Al-1Zn Alloy with Ultrafine Grained Structure[J]. Rare Metal Materials and Engineering,2014,43(11):2824~2828.]
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  • 收稿日期:2013-11-18
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  • 在线发布日期: 2015-04-07
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