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热处理对挤压铸造n-SiCp/AZ91D镁基复合材料组织和力学性能的影响
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清华大学自主科研计划(20111080980);国家高技术研究发展计划(“863”计划)项目(2013AA031201)


Effect of Heat Treatment on Microstructure and Mechanical Properties
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    摘要:

    采用金相、X射线衍射、扫描电镜(SEM)、拉伸试验等方法分析和测试了挤压铸造纳米SiC颗粒增强AZ91D镁基复合材料在铸态(F)、固溶态(T4)和人工时效态(T6)下的组织和力学性能。结果表明,固溶处理可使n-SiCp/AZ91D铸态组织中的β-Mg17Al12共晶相溶入到基体中,形成单一的过饱和α-Mg固溶体,合金抗拉强度和伸长率均有大幅提高,分别达到265 MPa 和13.7%;经时效处理后,复合材料的抗拉强度和屈服强度进一步提高,分别为275,145 MPa;SEM结果显示,β-Mg17Al12相主要以连续析出/非连续析出方式分别在晶内及晶界上析出,特别是纳米SiC颗粒分布对二次析出相β-Mg17Al12的形貌、尺寸、分布有一定的影响,使二次析出相变得细小和弥散分布,从而充分发挥了二次析出相的沉淀强化作用;最后对n-SiCp/AZ91D复合材料不同热处理条件下的断口形貌进行了SEM观察,并且对其断裂方式进行了分析和讨论

    Abstract:

    Magnesium matrix composite reinforced with SiC nanoparticles (n-SiCp/AZ91D) was fabricated by squeeze casting. The microstructure and mechanical properties of the nanocomposite at as-cast state (F), solid solution state (T4) and artificial aging state (T6) were investigated by optical microscopy, X-ray diffraction, scanning electronic microscopy (SEM) and tensile tests. The results show that the solid solution treatment can dissolve the β-Mg17Al12 eutectic phase in the matrix of n-SiCp/AZ91D composites to produce single supersaturated solid solution α-Mg phase and the ultimate tensile strength and elongation are significantly improved which can be up to 265 MPa and 13.7%, respectively. After aging treatment, the ultimate tensile strength and yield strength of the nanocomposite are further improved, which is 275 MPa and 145 MPa, respectively. SEM results show that the β-Mg17Al12 phase is mainly precipitated in grain and at grain boundary as continuous or non continuous forms. In particular SiC nanoparticles have an important effect on the morphology, size and distribution of the β-Mg17Al12 precipitation phase and they result in the fine and uniformly dispersed secondary precipitate phase to be formed, which gives full play to the secondary precipitation strengthening effect. Finally, the fracture morphology of n-SiCp/AZ91D composites at different heat treatment conditions were observed by SEM and the fracture behavior were analyzed and discussed

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张从阳,冯荣宇,李文珍.热处理对挤压铸造n-SiCp/AZ91D镁基复合材料组织和力学性能的影响[J].稀有金属材料与工程,2015,44(2):463~468.[Zhang Congyang, Feng Rongyu, Li Wenzhen. Effect of Heat Treatment on Microstructure and Mechanical Properties[J]. Rare Metal Materials and Engineering,2015,44(2):463~468.]
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  • 收稿日期:2014-01-15
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  • 在线发布日期: 2015-05-29
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