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固相块中微纳尺度Gd211粒子的控制及其对单畴GdBCO超导块材性能的影响
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陕西师范大学物理与信息技术学院,陕西师范大学物理与信息技术学院

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国家自然科学基金(项目号51572164, 51342001)、教育部科学技术研究重大项目(311033)、高等学校博士学科点专项科研基金(20120202110003)、陕西省重点科技创新团队项目(2014KTC-18)、中央高校基本科研业务费专项资金(GK201101001, GK201305014)资助


Effect of the microstructure of Gd211 particles on the levitation force of single domain GdBCO bulks by TSIG process
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College of Physics and information Technology,Shaanxi Normal University,Xi’an,College of Physics and information Technology,Shaanxi Normal University,Xi’an

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    摘要:

    通过控制Gd211固相块烧结温度的方法,获得了系列具有不同显微组织结构的Gd211先驱固相块;在此基础上,采用顶部籽晶熔渗生长法,制备了系列单畴GdBCO超导块材。并对其熔渗生长前后之宏观形貌、显微组织结构、以及单畴GdBCO超导块材的磁悬浮力进行了研究。结果表明,只有当先驱固相块的微观结构满足:Gd211粒子均为球状或椭球状颗粒、平均粒径较小、气孔率适中的条件时,单畴GdBCO超导块材中的Gd211粒子平均粒径最小,样品的磁通钉扎力和磁悬浮力最大(约38.7 N,样品直径20 mm,测试温度77 K,永磁体直径20 mm,表面磁场0.5 T)。该研究结果对于如何从微观结构上控制固相先驱块和单畴REBCO超导块材中RE211粒子的形状、粒径大小、气孔率、以及提高其超导性能提供了科学的依据和思路。

    Abstract:

    By controlling the sintering temperature of Gd211 solid pellet, a series of Gd211 precursors with different microstructures were obtained. On this basis, Single domain GdBCO bulk superconductors have been successfully fabricated by the top-seeding melt infiltration growth process. Through observing the macro morphology and microstructure of the GdBCO bulk and the Gd211 precursors, as well as measuring the magnetic levitation force of GdBCO superconductor, the results show that It was only when the microstructure of the precursors block meet conditions: Gd211 particles are spherical or ellipsoidal and the average size is smaller. The gaps between Gd211 particles are appropriate. The size of Gd211 particles in the single domain GdBCO bulk superconductor is the smallest, The magnetic flux pinning and levitation force of the sample is the largest(The maximum force is 38.7N, The sample diameter is 20mm, The test temperature is 77K, The permanent magnet diameter is 20mm,The surface magnetic field is 0.5T). The results provide scientific basis and ideas to improve the superconducting properties of HTS.

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渊小春,杨万民.固相块中微纳尺度Gd211粒子的控制及其对单畴GdBCO超导块材性能的影响[J].稀有金属材料与工程,2018,47(5):1613~1619.[Yuan Xiao-Chun, Yang Wan-min. Effect of the microstructure of Gd211 particles on the levitation force of single domain GdBCO bulks by TSIG process[J]. Rare Metal Materials and Engineering,2018,47(5):1613~1619.]
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  • 收稿日期:2016-04-26
  • 最后修改日期:2016-07-08
  • 录用日期:2016-08-17
  • 在线发布日期: 2018-06-08
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