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Al2O3陶瓷/AgCuTi/GH99高温合金的钎焊接头力学性能
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中国核动力研究设计院

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中国核动力研究设计院院青年基金


Mechanical properties of alumina ceramic/AgCuTi/GH99 superalloy brazed joints
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Nuclear Power Institute of China

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    摘要:

    采用AgCuTi钎料对Al2O3陶瓷与GH99高温合金进行了钎焊连接,研究了工艺参数(连接温度、保温时间)的变化对接头力学性能的影响,并分析了不同参数下接头的断裂位置,结果表明:保温5min时,在不同的连接温度下进行钎焊,随着连接温度的升高,接头的抗剪强度先增后减,在900℃时取得最大值,为127.24MPa,连接温度较低时,主要断裂于Al2O3/钎料侧,随着温度的升高,接头TiNi3反应层增厚,因此还有部分断裂于TiNi3反应层/钎料界面;在连接温度为900℃时,随着保温时间的延长,接头的抗剪强度逐渐降低,保温时间较短时,主要要断裂于Al2O3/钎料界面,保温时间过长,TiNi3反应层延伸入钎料中部且厚度大大增加,在该反应层中产生微裂纹,造成接头强度大大降低,此时部分断裂于钎料中部及TiNi3反应层中。

    Abstract:

    The Al2O3 ceramic was brazed to GH99 superalloy using AgCuTi filler alloy, The influence of the process parameters on the mechanical property of the joints was studied and the fracture location of joints under different process parameters was analysed. The results show that, With the increasing of brazing temperature, the shear strength of joints decreased after increasing to a maximum, The maximum was obtained at 900℃,Which is 127.24MPa. When the brazing temperature is lower, the fracture is mostly in Al2O3/filler side, With the increasing of brazing temperature, The TiNi3 reaction layer is gradually thickening and then parts of the fracture is in the TiNi3 reaction layer/filler interface; At 900℃, With the extension of the holding time, The shear strength of joint gradually decreased. The joints is mainly fractured in the Al2O3 ceramic/filler interface when the holding time is short. When the holding time is too long, the reaction layer extends into the middle of the solder and the thickness of TiNi3 layer is greatly increased, and the micro crack is produced in the reaction layer, Which cause the strength of the joint greatly reduced, And then the joint is partly fractured in the filler metal and TiNi3 reaction layer.

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叶晓凤,王宇,张恒泉,樊宝全,马新光,范永明. Al2O3陶瓷/AgCuTi/GH99高温合金的钎焊接头力学性能[J].稀有金属材料与工程,2018,47(11):3564~3570.[Ye Xiaofeng, Wang Yu, Zhang Hengquan, Fan Baoquan, Ma Xinguang, Fan Yongming. Mechanical properties of alumina ceramic/AgCuTi/GH99 superalloy brazed joints[J]. Rare Metal Materials and Engineering,2018,47(11):3564~3570.]
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  • 收稿日期:2017-01-24
  • 最后修改日期:2017-10-11
  • 录用日期:2017-11-09
  • 在线发布日期: 2018-12-19
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