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变形参数对TA32合金的超塑性变形行为及微观组织演化的影响
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1.清华大学机械工程系;2.北京星航机电装备有限公司

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中图分类号:

TG146.2

基金项目:

国家自然科学基金资助(51471090)


Effects of deformation parameters on the microstructure evolution and superplastic behavior of TA32 alloy
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1.Department of Mechanical Engineering,Tsinghua University;2.Beijing Xinghang Electro-mechanical Equipment Co,Ltd

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    摘要:

    针对我国自主研制的TA32高温钛合金,开展了在变形温度为895-935℃和应变速率为8.3×10-4-1.32×10-2 s-1条件下的高温拉伸变形试验研究,利用电子背散射技术(EBSD)表征了不同变形条件下的晶粒形貌、晶粒取向和分布规律。结果表明:TA32合金具有良好的超塑性变形能力,最大断裂延伸率能达到1141.8%。在高温和低应变速率条件下,晶粒的长大容易造成在变形后期真实应力出现上升现象。真实应力和断裂延伸率对变形温度、变形程度和应变速率均是敏感的,动态再结晶容易在高温或低应变速率条件下发生。动态再结晶程度随着变形温度的升高、应变速率的降低和变形程度的增大而增大,变形后的织构接近随机取向织构,原始晶粒得到等轴化,提高了晶粒尺寸的均匀性。在变形过程中,不连续动态再接晶是主要的动态再结晶机制,随着变形温度的升高、应变速率的降低和变形程度的增大,不连续动态再结晶的作用在增强,连续动态再结晶的作用则是在减弱。

    Abstract:

    High-temperature tensile test at a deformation temperature of 895-935℃ and a strain rate of 8.3×10-4-1.32×10-2 s-1 is conducted for TA32 high-temperature titanium alloy developed independently by our country, and electron back-scattered diffraction (EBSD) technique is used to characterize grain morphology, orientation, and grain distribution. The results show that TA32 alloy provides superior superplastic deformation capability, with a maximum fracture elongation up to 1141.8%. In high temperature and low strain rate conditions, growth of grains tends to result in the rise of true stress in late deformation stages. Both the true stress and fracture elongation are sensitive to deformation temperature, deformation degree, and strain rate. Dynamic recrystallization is more likely to occur in high temperature or low strain rate conditions. The degree of dynamic recrystallization increases with the increasing deformation temperature, the decrease of strain rate, or the increase of deformation degree. After deformation, the textures nearly exhibit random orientations, and the original grains get equiaxed with better dimensional uniformity. During the process of deformation, discontinuous dynamic recrystallization serves as the dominant dynamic recrystallization mechanism. With the increase of deformation temperature, decrease of strain rate, or increase of deformation degree, discontinuous dynamic recrystallization plays a more important role, while continuous dynamic recrystallization weakens.

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刘章光,李培杰,尹西岳,仵凤勇,熊亮同,高海涛.变形参数对TA32合金的超塑性变形行为及微观组织演化的影响[J].稀有金属材料与工程,2018,47(11):3473~3481.[Liu Zhangguang, Li Peijie, Yin Xiyue, Wu Fengyong, Xiong Liangtong, Gao Haitao. Effects of deformation parameters on the microstructure evolution and superplastic behavior of TA32 alloy[J]. Rare Metal Materials and Engineering,2018,47(11):3473~3481.]
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历史
  • 收稿日期:2017-03-16
  • 最后修改日期:2017-04-04
  • 录用日期:2017-04-14
  • 在线发布日期: 2018-12-19
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