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超细晶工业纯锆的室温蠕变特性及断口分析
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西安建筑科技大学冶金工程学院

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国家自然科学基金(51474170)、陕西省自然科学基金(2016JQ5026)和陕西省教育厅重点实验室科研计划项目(15JS058)联合资助


Creep Behavior and Fracture of Ultra-Fine Grained Commercial Purity Zirconium at Ambient Temperature
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1.School of Metallurgical Engineering, Xi''an University of Architecture and Technology;2.Xi''an Uninversity of Architecture and Technology

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    摘要:

    本文分别研究了超细晶工业纯锆在 0.875 Rp0.2、0.9 Rp0.2、0.9125 Rp0.2、0.925 Rp0.2、0.9375 Rp0.2、0.95 Rp0.2蠕变应力下的室温蠕变性能,计算了超细晶工业纯锆的稳态蠕变速率,并分析了其蠕变断裂机理。实验结果表明:超细晶工业纯锆在蠕变应力为0.875 Rp0.2时,出现了蠕变饱和现象,稳态蠕变速率随着蠕变应力的增加而增大,稳态蠕变阶段缩短;当蠕变应力为0.95 Rp0.2时,稳态蠕变速率达到最大值3.140×10-6s-1。通过计算蠕变应力指数,得到超细晶工业纯锆的室温蠕变机理为位错运动。超细晶工业纯锆室温蠕变断裂为韧性断裂。

    Abstract:

    The creep tests were carried out on Ultra-fine grained commercial purity zirconium under the stresses of 0.875 Rp0.2、0.9 Rp0.2、0.9125 Rp0.2、0.925 Rp0.2、0.9375 Rp0.2、0.95 Rp0.2 at ambient temperature. Steady state creep rate was calculated. The creep fracture of UFG CP Zr was investigated by SEM. A new expression was proposed which fit the creep of UFG CP Zr better. It was found that the creep saturation phenomenon happened under 0.875 Rp0.2; the steady state creep rate increased with the rise of creep stress which led the steady state creep stage shortening; the maximum of steady state creep rate was 3.140×10-6s-1 under 0.95 Rp0.2. According to the calculated creep stress exponent, the creep mechanism can be categorized into the dislocation motion. The creep fracture of UFG CP Zrwas ductile fracture.

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杨西荣,朱振,刘晓燕,罗雷,赵西成.超细晶工业纯锆的室温蠕变特性及断口分析[J].稀有金属材料与工程,2019,47(3):815~819.[YANG XIRONG, ZHU ZHEN, LIU XIAOYAN, LUO LEI, ZHAO XICHENG. Creep Behavior and Fracture of Ultra-Fine Grained Commercial Purity Zirconium at Ambient Temperature[J]. Rare Metal Materials and Engineering,2019,47(3):815~819.]
DOI:10.12442/j. issn.1002-185X.20170641

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  • 收稿日期:2017-07-20
  • 最后修改日期:2017-09-26
  • 录用日期:2017-10-12
  • 在线发布日期: 2019-04-10
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