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降温往复镦粗-挤压变形对Mg-Gd-Y-Zn-Zr合金晶粒细化及织构变化的研究
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中北大学材料科学与工程学院,中北大学材料科学与工程学院,中北大学材料科学与工程学院,中北大学材料科学与工程学院,中北大学材料科学与工程学院

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Study on Grain Refinement and Texture Evolution of Mg-Gd-Y-Zn-Zr alloy processed by Repetitive Usetting-extrusion at decreasing temperature
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School of Material Science and Engineering,North University of China,School of Material Science and Engineering,North University of China,School of Material Science and Engineering,North University of China,School of Material Science and Engineering,North University of China,School of Material Science and Engineering,North University of China

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    摘要:

    本文在480°C降温至370°C条件下,采用循环镦?挤工艺对均匀化后的Mg-Gd-Y-Zn-Zr合金进行变形,对循环镦?挤变形过程中的合金微观组织和织构变化进行研究。结果表明,随着循环镦?挤变形道次的增加,晶粒尺寸逐渐减小。在变形6道次后,累积应变达到 8.4,得到了平均晶粒尺寸为 3.4 μm 的细小均匀的微观组织。晶粒细化是由非连续动态再结晶和连续动态再结晶复杂共同作用引起的。另外,变形过程中,原始粗大晶粒内的片层状长程有序相(LPSO)发生扭折变形产生扭折带,并在扭着带处引起动态再结晶产生,分割原始粗晶,起到晶粒细化作用。结果还表明,一道次镦?挤变形后,合金产生强的基面织构,随着变形道次的增加,织构强度有所减弱。织构弱化的原因是动态再结晶和加载力在轴向和径向交替变化共同作用。

    Abstract:

    A homogenized Mg-13Gd-4Y-2Zn-0.5Zr (wt.%) alloy was subjected to repetitive upsetting-extrusion (RUE) process at decreasing temperature from 480 to 370℃. The microstructure and texture development of the alloy during the RUE process was investigated in current study. The results showed that average grain size decreased with increasing cumulative strain and decreasing temperature. Uniform ultrafine-grain structure with an average grain size of 3.4 μm was achieved after 6 passes, i.e., cumulative strain of 8.4. Results revealed that grain refinement was induced by a complicated combination of discontinuous dynamic recrystallization and continuous dynamic recrystallization. Kink of lamellar long period stacking order (LPSO) phases played an important role in the grain refinement through subdividing the coarse grains by inducing recrystallization evolved in the kink bands. After 1 pass of RUE, a strong basal texture was obtained. With increasing RUE passes, the texture was gradually weakened, which resulted from cooperative effect of DRX and the alternative change of loading directions (axial and radial) during RUE processing.

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张治民,杜玥,张冠世,于建民,闫钊鸣.降温往复镦粗-挤压变形对Mg-Gd-Y-Zn-Zr合金晶粒细化及织构变化的研究[J].稀有金属材料与工程,2018,47(5):1422~1428.[Zhang Zhimin, Du Yue, Zhang Guanshi, Yan Zhaoming, Yu Jianmin. Study on Grain Refinement and Texture Evolution of Mg-Gd-Y-Zn-Zr alloy processed by Repetitive Usetting-extrusion at decreasing temperature[J]. Rare Metal Materials and Engineering,2018,47(5):1422~1428.]
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  • 收稿日期:2017-10-19
  • 最后修改日期:2017-12-12
  • 录用日期:2017-12-15
  • 在线发布日期: 2018-06-08
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