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离心雾化制备SAC305球形粉工艺研究
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1.昆明理工大学材料科学与工程学院;2.云南锡业锡材有限公司

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云南省重大专项(项目号2018ZE004)


Production of SAC305 Solder Powder by Rotating Atomization Disk
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    摘要:

    为生产高质量的SAC305合金球形粉末,研究了转速、处理量、雾化器形状、气氛含氧量等工艺参数对旋转离心雾化生产Sn-3.0Ag-0.5Cu粉末性能的影响。结果表明随着转速(6000-60000rpm)的提高、进料量(30-60kg/h)的降低和雾化器尺寸(30-50mm)的增大,SAC305粉末平均粒径变小,CFD模拟与实验有一致的趋势,实验修正因子n为1.65,CFD模拟修正因子为2.23。杯形雾化盘相比平面雾化盘生产的粉末平均粒径降低了8%。SEM照片显示,随着雾化室氧含量的降低,粉末球形度提高,雾化室中的含氧量低于400ppm时,粉末表面含氧量低于100 ppm,雾化室与熔体的温差在230℃时粉末表面质量较好。SAC305粉末粒径和球形度主要受工艺控制,粉体表面质量与冷却效率和收集技术有关。

    Abstract:

    In order to produce high-quality SAC305 alloy spherical powder, we studyed the effects of operating parameters: rotating speed, melt feed rate, shape and size of atomizer, and oxygen content in the atomizer chamber on the performance to produce Sn-3.0Ag-0.5Cu powder by rotary centrifugal atomization. It was evidenced from the experimental results that the median size of the atomized powders became smaller with increasing rotating speed(6000-60000rpm), decreasing melt feed rate(30-60kg/h the ), and use of larger atomizer(30-50mm), the experiment value of n is 1.65,the CFD value of n is 1.65. A cup shaped atomizer was able to give approx. 8% finer powder compared to that from a flat-disk shaped one. SEM micrographs revealed that the oxygen content of the atomization chamber decreased, the powder sphericity factor approached 1. When the oxygen content in the atomization chamber was less than 400 ppm, the oxygen content on the powder surface was less than 100 ppm. The surface quality is the best when the superheat of the atomization chamber and the melt is 230℃, the atomization parameters control the particle size and sphericity of the powder. SAC305 powder particle size and sphericity are mainly controlled by the process, and the powder surface quality is related to the cooling efficiency and collection technology.

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陇赞,白海龙,陈东东,段雪霖,严继康,*易健宏.离心雾化制备SAC305球形粉工艺研究[J].稀有金属材料与工程,2021,50(9):3313~3319.[Long Zan, Bai Hailong, Chen Dongdong, Duan Xueling, Yan Jikang, Yi Jianhong. Production of SAC305 Solder Powder by Rotating Atomization Disk[J]. Rare Metal Materials and Engineering,2021,50(9):3313~3319.]
DOI:10.12442/j. issn.1002-185X.20200728

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历史
  • 收稿日期:2020-09-19
  • 最后修改日期:2021-01-20
  • 录用日期:2021-02-03
  • 在线发布日期: 2021-09-27
  • 出版日期: 2021-09-24