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Nb对钠冷快堆包壳用15-15Ti奥氏体不锈钢组织和拉伸性能的影响
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1.东北大学 材料科学与工程学院;2.中国科学院金属研究所 核用材料与安全评价重点实验室;3.中国原子能科学研究院;4.中国科学院核用材料与安全评价重点实验室中国科学院金属研究所

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Effect of niobium content on the microstructure and tensile properties of 15Cr-15Ni Titanium-modified Austenitic Stainless Steel used as core components in liquid metal-cooled fast reactors (LMFR).
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    摘要:

    使用OM、SEM和TEM等方法研究了0~0.46wt.%Nb对固溶态和时效态15Cr-15Ni含Ti奥氏体不锈钢(15-15Ti)中析出相类型、形貌及其分布的影响。结果表明,Nb取代了(Ti,Mo)C相中部分Ti、Mo原子,在0.21wt.%Nb和0.46wt.%Nb合金中形成富Nb的(Nb,Ti)C相,而且Nb含量的增加使固溶态的奥氏体基体组织细化。在850 ℃时效1000h后,组织中有sigma相、MC碳化物析出,Nb的增加促进了 Nb、Mo元素在sigma相中的富集,促使sigma相更为细小、弥散析出。固溶态和时效态试样的室温、650 ℃拉伸结果表明,在0~0.46 wt.% Nb范围内,Nb含量的增加对固溶态合金室温和高温拉伸性能影响较小,而Nb促进析出的sigma相对时效态合金的拉伸性能影响较小。

    Abstract:

    This study investigated the precipitated phases of Titanium-stabilized 15Cr-15Ni austenitic stainless steel with different niobium contents (0-0.46 wt.%), in which the types, morphology and distribution of precipitated phases after solution treatment and aging treatment were characterized by means of OM, SEM, and TEM. Results show that Ti and Mo can be partly replaced with Nb in (Ti,Mo)C phase to form a Nb-rich (Nb,Ti)C phase in 0.21wt.%Nb and 0.46wt.%Nb alloys. What’s more , the increase of Nb content refines austenite matrix structure after solution treatment. In addition , the main phases in the alloy after aging at 850℃ for 1000h are sigma and MC carbides .the increase of Nb content not only promotes to enrich Nb and Mo elements in the sigma phases, but also furthers it to be finer and dispersed. Besides, in the range of 0-0.46wt.%Nb, the tensile results of solution and aged specimens at room temperature and 650℃ show that the increase of Nb content has little effect on the tensile properties of the solution alloy at room temperature and high temperature, while the sigma promoted by Nb has no effect on the tensile properties of the aged alloy.

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乔羽飞,陈思含,任媛媛,梁田,刘春明,马颖澈,刘奎. Nb对钠冷快堆包壳用15-15Ti奥氏体不锈钢组织和拉伸性能的影响[J].稀有金属材料与工程,2021,50(11):4079~4088.[Yufei Qiao, Sihan Chen, Yuanyuan Ren, Tian Liang, Chunming Liu, Yinche Ma, Kui Liu. Effect of niobium content on the microstructure and tensile properties of 15Cr-15Ni Titanium-modified Austenitic Stainless Steel used as core components in liquid metal-cooled fast reactors (LMFR).[J]. Rare Metal Materials and Engineering,2021,50(11):4079~4088.]
DOI:10.12442/j. issn.1002-185X.20200900

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历史
  • 收稿日期:2020-11-22
  • 最后修改日期:2020-12-14
  • 录用日期:2020-12-23
  • 在线发布日期: 2021-11-30
  • 出版日期: 2021-11-24