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固溶时效处理对TC11钛合金组织与 冲击性能的影响
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大连交通大学 连续挤压教育部工程研究中心

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中图分类号:

TG156.1

基金项目:

国家自然科学基金资助项目(51675074);辽宁省教育厅项目(JDL2019001);大连市科技创新基金资助项目(2018J11CY027)


(05):768.

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Affiliation:

Engineering Research Center of Continuous Extrusion,Ministry of Education,Dalian Jiaotong University

Fund Project:

Funded by the National Natural Science Foundation of China ( 51675074 ) ; liaoning Provincial Department of Education Project ( JDL2019001 ) ; dalian Science and Technology Innovation Fund Project ( 2018J11CY027 )

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    摘要:

    对TC11钛合金棒材进行固溶时效处理,通过光学显微镜、XRD以及冲击性能测试等,研究固溶时效处理后该合金微观组织与冲击性能的关系。结果表明:两相区固溶处理后,组织变化较小,时效后组织中出现β转变组织,并有α′相析出,单相区固溶处理后,初生α相完全消失,α′相数量和尺寸随着时效时间增加而增加,出现晶界β相;两相区固溶后,组织由α相与α″相构成,单相区固溶后,组织由α′相与α″相构成,当进行时效处理后,组织均由α相和β相构成;棒材的冲击韧性在单相区固溶处理后最大,最大值为22 J/cm2,两组冲击韧性值均是随着时效温度升高而降低,但降低幅度较小;两相区固溶后的裂纹扩展路径较为平缓,经时效后裂纹路径产生偏折,而单相区固溶后的裂纹扩展路径曲折程度较大,再经时效处理后的裂纹发生巨大偏转,扩展路径更加曲折。

    Abstract:

    The TC11 titanium alloy bar was subjected to solution aging treatment, and the relationship between the microstructure and impact properties of the alloy after solution aging treatment was studied by optical microscopy, XRD and impact performance testing. The results show that after the solution treatment in the two-phase region, the microstructure changes are small, and the β-transition structure appears in the structure after aging, and the α" phase is precipitated. After the solution treatment in the single-phase region, the primary α phase completely disappears, and the number of α" phases The grain boundary β phase appears; After solid solution in two-phase region, the microstructure consists of α phase and α′′ phase. After solid solution in single-phase region, the microstructure consists of α′ phase and α′′ phase. After aging treatment, the microstructure consists of α phase and β phase.; the impact toughness of the bar is the largest after solution treatment in the single-phase region, and the maximum value is 22 J /cm2, the impact toughness values of the two groups decreased with the increase of the aging temperature, but the decrease range was small; the crack propagation path after solid solution in the two-phase region was relatively gentle, and the crack path was deflected after aging, while the single-phase The crack propagation path after solid solution in the zone is more tortuous, and the crack after aging treatment is greatly deflected, and the propagation path is more tortuous.

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引用本文

张明玉,运新兵.固溶时效处理对TC11钛合金组织与 冲击性能的影响[J].稀有金属材料与工程,2023,52(5):1759~1766.[Zhang Mingyu, Yun Xinbing.(05):768.


DOI:10.12442/j. issn.1002-185X.20220310

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历史
  • 收稿日期:2022-04-14
  • 最后修改日期:2022-06-29
  • 录用日期:2022-07-12
  • 在线发布日期: 2023-06-08
  • 出版日期: 2023-05-29