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热处理对一种抗热腐蚀单晶高温合金组织和持久性能的影响
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作者单位:

1.中国科学院金属研究所;2.辽宁科技大学机械工程与自动化学院

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中图分类号:

TG146.1+5

基金项目:

国家重点研发计划(2021YFC2202402);辽宁省科技攻关计划课题(2019JH2/10100009)


Effect of Heat Treatment on Microstructures and Stress Rupture Properties of a Hot-Corrosion Resistant Single Crystal Superalloy
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Affiliation:

1.Institute of Metal Research, Chinese Academy of Sciences;2.School of Mechanical Engineering and Automation, University of Science and Technology Liaoning

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    摘要:

    研究了热处理对一种抗热腐蚀单晶高温合金微观组织及1070 ℃/140 MPa持久性能的影响。结果表明:长时间的均匀化热处理显著降低了元素偏析;随着均匀化时间的延长,微孔面积分数逐渐增加,平均尺寸不断增大,微孔的密度呈先升高后降低的变化趋势;随一级时效温度的升高,γ′相尺寸逐渐增大,γ′相面积分数先增加后减少;合金的持久寿命随一级时效温度的提高先升高后降低,一级时效温度为1100 ℃时,立方状γ′相尺寸约370 nm且正方度较好,γ′相的面积分数最大,持久寿命最高;持久断口具有韧性断裂特征,亚晶界处的碳化物和微孔是引起持久试样断裂的主要裂纹源。

    Abstract:

    The effects of heat treatment on the microstructures and rupture properties at 1070 ℃/140 MPa of a hot-corrosion resistant single crystal superalloy was investigated. The results show that long-term homogenization heat treatment significantly reduces element segregation. With the extension of homogenization time, the area fraction of micropores gradually increases, the average size keeps increasing, and the density of micropores increases firstly and then decreases. With the increase of primary aging temperature, the size of γ" phase enlarge gradually, the area fraction of γ" phase frist increases and then decreases. The stress rupture life of the alloy increases first and then decreases with the increase of the primary aging temperature. When the primary aging temperature is 1100 ℃, the size of the cubic γ" phase is about 370 nm and the squareness is better, the area fraction of the γ" phase is the largest and the stress rupture life is the highest. The stress rupture fracture is characterized by ductile fracture. The carbides and micropores at the sub-grain boundary are the main crack sources that cause the stress rupture fracture of the sample.

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来永军,宁礼奎,柳一川,刘恩泽,孟祥伦,谭政,佟健,郑志.热处理对一种抗热腐蚀单晶高温合金组织和持久性能的影响[J].稀有金属材料与工程,2023,52(6):2243~2252.[laiyongjun, ninglikui, liuyichuan, liuenze, mengxianglun, tanzheng, tongjian, zhengzhi. Effect of Heat Treatment on Microstructures and Stress Rupture Properties of a Hot-Corrosion Resistant Single Crystal Superalloy[J]. Rare Metal Materials and Engineering,2023,52(6):2243~2252.]
DOI:10.12442/j. issn.1002-185X.20220589

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  • 收稿日期:2022-07-15
  • 最后修改日期:2022-10-25
  • 录用日期:2022-11-09
  • 在线发布日期: 2023-07-07
  • 出版日期: 2023-06-30