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固溶处理工艺对一种镍基单晶高温合金长期时效后持久性能的影响
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1.中国科学院金属研究所师昌绪先进材料创新中心高温结构材料研究部;2.东北大学轧制技术及连轧自动化国家重点实验室

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Effect of solution treatment on creep rupture properties after long-term aging of a Nickel-based single crystal superalloy
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1.Shi-Changxu Innovation Center for Advanced Materials,Institute of Metal Research,Chinese Academy of Sciences;2.The State Key Laboratory of Rolling and Automation,Northeastern University

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    摘要:

    本文通过对一种传统镍基单晶高温合金在不同热处理工艺条件下的固溶和时效进行实验,研究了固溶时间和长期时效对合金微观组织和性能的影响。结果表明:镍基单晶高温合金较佳的热处理工艺为1310℃/4h(空冷)+1130℃/4h(空冷)+899℃/16h(空冷)。经过固溶处理后,极大程度避免析出不利TCP相,获得尺寸较小、立方度较高的强化相γ′的微观组织。不同热处理制度下,合金持久断裂寿命和延展率相差较小。变形过程中,脆性针状TCP相优先破碎,不是裂纹萌生处。而枝晶间的薄弱的碳化物/基体界面提供了裂纹的源头。

    Abstract:

    In this research, the effects of solution time and long-term aging on microstructure evolution and mechanical properties of a traditional nickel-based single crystal superalloy under different heat treatment conditions were studied. The obtained results demonstrate that the best heat treatment regime is “1310℃/4h (AC)+1130℃/4h (AC)+899℃/16h (AC)”. After the solution treatment, the participating of adverse phase of TCP has been avoided to obtain the preferable microstructure with small size and a high degree of cubic of strengtheningγ′phase. The difference in creep rupture life and percentage of elongation is slight under different heat treatment regimes. During the deformation, the brittle TCP phase was broken first, demonstrating that it is not the crack initiation. However, the weak carbide/matrix interface in inter-dendrites is the source of the crack.

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王楠,刘纪德,朱崇伟,张志鹏,徐伟,李金国.固溶处理工艺对一种镍基单晶高温合金长期时效后持久性能的影响[J].稀有金属材料与工程,2024,53(11):3129~3135.[Nan Wang, Jide Liu, Congwei Zhu, Zhipeng Zhang, Wei Xu, Jinguo Li. Effect of solution treatment on creep rupture properties after long-term aging of a Nickel-based single crystal superalloy[J]. Rare Metal Materials and Engineering,2024,53(11):3129~3135.]
DOI:10.12442/j. issn.1002-185X.20230532

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历史
  • 收稿日期:2023-08-30
  • 最后修改日期:2024-01-04
  • 录用日期:2024-01-05
  • 在线发布日期: 2024-11-20
  • 出版日期: 2024-11-08