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电子束熔炼对DZ125合金返回料夹杂物分布的影响研究
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作者单位:

北京北冶功能材料有限公司,北京 100192

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中图分类号:

TG146.15

基金项目:

国家重点研发计划(2022YFB3705003);航空发动机及燃气轮机重大专项基础研究项目(J2019-VI-0010-0124)


Influence of Electron Beam Melting on Distribution of Inclusions in DZ125 Superalloy Revert
Author:
Affiliation:

Beijing Beiye Functional Materials Co., Ltd, Beijing 100192, China

Fund Project:

National Key R&D Program of China (2022YFB3705003)

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    摘要:

    含铪铸造高温合金由于其返回料中氧化铪等夹杂物比重大,使用传统方法难以去除,本实验使用高能电子束对DZ125合金返回料进行熔炼,并对电子束精炼后的铸锭顶部、内部以及炉膛内收集的料渣成分、形貌及夹杂物分布进行分析。结果表明铸锭最后凝固区表面主要含有大尺寸氧化物夹杂及MC碳化物,铸锭内部不同位置均未发现氧化物夹杂,炉膛内料渣存在大尺寸HfO2。高能电子束对熔池起到搅拌作用,使HfO2和Al2O3在电子束作用下大量聚集上浮到铸锭表面,有效去除返回料内部的难熔氧化物。

    Abstract:

    Due to the large proportion of the inclusions, it''s hard to remove the inclusions such as hafnium oxide in the cast superalloy containing hafnium. In this research, DZ125 superalloy revert was melted by high energy electron beam to remove refractory inclusion, and the composition, microstructure and distribution of slag collected from different positions after electron beam melting were analyzed. The results show that the surface of the final zone of the ingot mainly contains large-sized oxide inclusions and MC carbides, no oxide inclusions are found in different positions inside the ingot, and large-sized HfO2 is found in the slag in the hearth. The high energy electron beam has a stirring effect on the molten pool, which makes a large number of HfO2 and Al2O3 gather together and float to the surface of the ingot under the action of the electron beam, so the refractory oxide inclusion in the revert can be effectively removed.

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黄丹蓝,薛佳宁,安宁,邬雅靓,石枫,曹合欢,杨帆,李重阳.电子束熔炼对DZ125合金返回料夹杂物分布的影响研究[J].稀有金属材料与工程,2025,54(5):1229~1234.[Huang Danlan, Xue Jianing, An Ning, Wu Yajing, Shi Feng, Cao Hehuan, Yang Fan, Li Chongyang. Influence of Electron Beam Melting on Distribution of Inclusions in DZ125 Superalloy Revert[J]. Rare Metal Materials and Engineering,2025,54(5):1229~1234.]
DOI:10.12442/j. issn.1002-185X.20230817

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历史
  • 收稿日期:2023-12-18
  • 最后修改日期:2024-03-28
  • 录用日期:2024-04-16
  • 在线发布日期: 2025-05-23
  • 出版日期: 2025-05-22