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含Gd不锈钢的时效处理及腐蚀行为
作者:
作者单位:

1.太原科技大学 材料科学与工程学院，山西 太原 030024;2.中国科学院金属研究所 沈阳材料科学国家研究中心，辽宁 沈阳 110016;3.中国科学院金属研究所 师昌绪先进材料创新中心，辽宁 沈阳 110016;4.中国科学技术大学 材料科学与工程学院，辽宁 沈阳 110016;5.中国科学院金属研究所 核用材料与安全评价重点实验室，辽宁 沈阳 110016

基金项目:

SYNL (L2019F15); Ling Chuang Research Project of China National Nuclear Corporation (CNNC-LCKY-202279)


Annealing Treatment and Corrosion Behavior of Gd-containing Stainless Steel
Author:
Affiliation:

1.School of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan 030024, China;2.Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;3.Shi-Changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;4.School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China;5.CAS Key Laboratory of Nuclear Materials and Safety Assessment, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Fund Project:

Research Foundation of Shenyang National Laboratory for Materials Science (L2019F15); Ling Chuang Research Project of China National Nuclear Corporation (CNNC-LCKY-202279)

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    摘要:

    研究了含1wt% Gd中子吸收双相不锈钢在不同温度时效后的微观结构与腐蚀行为。结果表明，材料中含Gd第二相的体积比以1080 ℃为转折点，先增后减。在1080 ℃时效处理的样品中，主要以第二相为双相M-Gd化合物（M=Fe，Cr，Ni），其核心为M3Gd相，外层为M12Gd相。在1140 ℃时效处理后，M3Gd为主要第二相。同时，研究了这两种样品在NaCl、HCl及H3BO3溶液中的腐蚀行为。1140 ℃处理后的样品具有相对较低的腐蚀速率。在NaCl和HCl溶液中，M3Gd较M12Gd具有较高的电化学活性；而在H3BO3溶液中，M3Gd则较为稳定。

    Abstract:

    The microstructures and corrosion behavior of 1.0wt% Gd-containing neutron-absorbing duplex stainless steel annealed at different temperatures were studied. Results reveal that the content of Gd-containing secondary phase increases with increasing the annealing temperatures to 1080 ℃, and then decreases. In the sample annealed at 1080 ℃, M-Gd (M=Fe, Cr, Ni) intermetallic with M3Gd as the core phase and M12Gd as the shell is the primary secondary phase. In the sample annealed at 1140 ℃, M3Gd phase is dominant. The corrosion behavior of the two annealed steel samples were analyzed in NaCl, HCl and H3BO3 solutions. It is found that the sample annealed at 1140 ℃ has lower corrosion rate. M3Gd is more electrochemically active than M12Gd when the sample is immersed in NaCl and HCl solutions, but more noble in H3BO3 solution.

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解曼曼,贾洞箫,贾茜霖,赵菲,梁田,周杨韬.含Gd不锈钢的时效处理及腐蚀行为[J].稀有金属材料与工程,2025,54(4):871~878.[Xie Manman, Jia Dongxiao, Jia Xilin, Zhao Fei, Liang Tian, Zhou Yangtao. Annealing Treatment and Corrosion Behavior of Gd-containing Stainless Steel[J]. Rare Metal Materials and Engineering,2025,54(4):871~878.]
DOI：10.12442/j. issn.1002-185X.20240115

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  • 收稿日期:2024-03-05
  • 最后修改日期:2025-03-18
  • 录用日期:2024-05-23
  • 在线发布日期: 2025-04-23
  • 出版日期: 2025-04-21

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