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电解铜的热变形行为及微观组织演变
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1.兰州理工大学 材料科学与工程学院,甘肃 兰州 730050;2.兰州理工大学 省部共建有色金属先进加工与再利用国家重点实验室,甘肃 兰州 730050;3.金川集团铜业有限公司,甘肃 金昌 737100

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TG306

基金项目:

甘肃省高等学校产业支撑计划项目(2022CYZC-19);甘肃省科技重大专项(22ZD6GA008)


Hot Deformation Behavior and Microstructure Evolution of Electrolytic Copper
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Affiliation:

1.School of Materials Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, China;2.State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou University of Technology, Lanzhou 730050, China;3.Jinchuan Group Copper Co., Ltd, Jinchang 737100, China

Fund Project:

Gansu Province Higher Education Institutions Industrial Support Program Project (2022CYZC-19); Gansu Provincial Science and Technology Major Project (22ZD6GA008)

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    摘要:

    在变形量70%的条件下,通过Gleeble-3500热模拟试验机研究了电解铜在500~800 ℃和0.01~10 s-1范围内的热变形行为。分析电解铜在热变形过程中各变形参数下的真应力-真应变曲线,建立了应变为0.5时的本构方程。在Prasad提出的动态材料模型基础上建立了不同应变下的加工图。同时,采用电子背散射对压缩后的试样进行微观组织观察与分析。结果表明:电解铜在高温塑性变形过程中对变形温度和应变速率表现出较强的敏感性,随着温度的升高和应变速率的降低,流变应力逐渐减小。根据加工图确定了电解铜的加工条件为变形温度600~650 ℃,应变速率5~10 s-1。电解铜在高温塑性变形过程中发生了不连续动态再结晶,在低温高应变速率下,晶粒明显细化。

    Abstract:

    The hot deformation behavior of electrolytic copper was investigated using a Gleeble-3500 thermal simulation testing machine at temperatures ranging from 500 °C to 800 °C and strain rates ranging from 0.01 s-1 to 10 s-1, under 70% deformation conditions. The true stress-true strain curves were analyzed and a constitutive equation was established at a strain of 0.5. Based on the dynamic material model proposed by Prasad, processing maps were developed under different strain conditions. Microstructure of compressed sample was observed by electron backscatter diffraction. The results reveal that the electrolytic copper demonstrates high sensitivity to deformation temperature and strain rate during high-temperature plastic deformation. The flow stress decreases gradually with raising the temperature and reducing the strain rate. According to the established processing map, the optimal processing conditions are determined as follows: deformation temperatures of 600–650 °C and strain rates of 5–10 s-1. Discontinuous dynamic recrystallization of electrolytic copper occurs during high-temperature plastic deformation, and the grains are significantly refined at low temperature and high strain rate conditions.

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张涵,桑晨,张燕,徐仰涛,乔及森,夏天东.电解铜的热变形行为及微观组织演变[J].稀有金属材料与工程,2025,54(4):920~929.[Zhang Han, Sang Chen, Zhang Yan, Xu Yangtao, Qiao Jisen, Xia Tiandong. Hot Deformation Behavior and Microstructure Evolution of Electrolytic Copper[J]. Rare Metal Materials and Engineering,2025,54(4):920~929.]
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历史
  • 收稿日期:2024-03-22
  • 最后修改日期:2025-04-11
  • 录用日期:2024-05-08
  • 在线发布日期: 2025-04-23
  • 出版日期: 2025-04-21