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显微组织对FGH4113A高温合金热变形行为和组织演变的影响
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1.深圳市万泽航空科技有限责任公司,广东 深圳 518000;2.中南大学 粉末冶金研究院,湖南 长沙 410083;3.深圳市万泽中南研究院有限公司,广东 深圳 518000

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深圳市科技计划资助 KJZD20230923113900001


Influence of Microstructures on Hot Deformation Behavior and Microstructure Evolution of FGH4113A Superalloy
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Affiliation:

1.Shenzhen Wedge Aviation Technology Co., Ltd, Shenzhen 518000, China;2.Powder Metallurgy Research Institute, Central South University, Changsha 410083, China;3.Shenzhen Wedge Central South Research Institute Co., Ltd, Shenzhen 518000, China

Fund Project:

Shenzhen Science and Technology Program (KJZD20230923113900001); Project of Industry and Information Technology Bureau of Shenzhen Municipality (201806071403422960)

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    摘要:

    研究了热等静压(HIP,A1)、热等静压+1100 ℃热挤压(A2)、热等静压+1150 ℃热挤压(A3)3种不同热变形条件下的热压缩曲线和变形组织。结果表明:1100 ℃挤压的A2样品具有均匀的γ+γ′双相细晶粒组织,1050和1100 ℃条件下均表现出良好的热变形性能。在较大应变范围内,A2样品的真应力-真应变曲线保持了硬化-软化平衡状态,变形后平均晶粒尺寸5 μm。热等静压态A1样品和1150 ℃挤压A3样品在1050 ℃仍处于变形软化阶段,组织为原始粗大晶粒和细小再结晶晶粒的混合项链晶,样品的再结晶形核机制主要为应变诱发晶界弓弯形核。1150 ℃?0.001 s-1条件下,初始组织对热变形行为和变形后组织的影响相对较小,变形后组织为完全再结晶的晶粒。细晶组织有利于最大化合金的热变形潜力。通过合理地调控变形机制,可以获得细小均匀的变形组织。

    Abstract:

    The hot compression curves and deformed microstructures were investigated under various hot deformation conditions in three states: hot isostatic pressing (HIP, A1), HIP+hot extrusion at 1100 ℃ (A2), and HIP+hot extrusion at 1150 ℃ (A3). The results show that A2 sample, extruded at 1100 ℃ with uniform γ+γ′ duplex microstructures, demonstrates excellent hot deformation behavior at both 1050 and 1100 ℃. The true stress-true strain curves of A2 sample maintain a hardening-softening equilibrium over a larger strain range, with post-deformation average grain size of 5 μm. The as-HIPed A1 sample and 1150 ℃ extruded A3 sample exhibit a softening region in deformation curves at 1050 ℃, and the grain microstructures reflect an incomplete recrystallized state, i.e. combination of fine recrystallized grains and initial larger grains, characterized by a necklace-like microstructure. The predominant recrystallization mechanism for these samples is strain-induced boundary migration. At 1150 ℃ with a strain rate of 0.001 s-1, the influence of the initial microstructure on hot deformation behavior and resultant microstructure is relatively less pronounced, and post-deformation microstructures are fully recrystallized grains. Fine-grained microstructures are conducive to maximizing the hot deformation potential of alloy. By judiciously adjusting deformation regimes, a fine and uniform deformed microstructure can be obtained.

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杨金龙,熊江英,尹超,程俊义,郭建政,冯赣江.显微组织对FGH4113A高温合金热变形行为和组织演变的影响[J].稀有金属材料与工程,2025,54(4):898~907.[Yang Jinlong, Xiong Jiangying, Yin Chao, Cheng Junyi, Guo Jianzheng, Feng Ganjiang. Influence of Microstructures on Hot Deformation Behavior and Microstructure Evolution of FGH4113A Superalloy[J]. Rare Metal Materials and Engineering,2025,54(4):898~907.]
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历史
  • 收稿日期:2024-04-03
  • 最后修改日期:2025-03-17
  • 录用日期:2024-07-08
  • 在线发布日期: 2025-04-23
  • 出版日期: 2025-04-21