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温度对真空热压连接技术制备AZ31/Al/Ta复合材料界面组织和力学性能的影响
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华北电力大学 先进材料研究院

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Effect of Temperature on the Interface Microstructure andMechanical Properties of AZ31/Al/Ta Composites Prepared by Vacuum Hot Compression Bonding
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1.Institute for Advanced Materials,North China Electric Power University;2.Beijing Institute of Spacecraft System Engineering

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National Natural Science Foundation of China (No.52275308; No.52301146), The Fundamental Research Funds for the Central Universities (2023JG007), and funding from Shi Changxu Innovation Center for Advanced Materials (SCXKFJJ202207).

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    摘要:

    Mg/Ta 复合材料兼具抗高能粒子辐照和轻质特性,这使其能够更好的满足未来深空探测需求。然而,由于这两种不同金属在性能上存在显著差异,将它们连接起来颇具挑战性。本文采用真空热压连接方法成功制备了AZ31/Al/Ta复合材料。研究了热压温度对AZ31/Al/Ta复合材料界面组织演变、相组成及界面剪切强度的影响。探讨了AZ31/Al/Ta复合材料在VHCB工艺条件下的界面结合机理。结果表明,随着热压温度的升高,Mg-Al界面相组成由Mg-Al脆性IMC(Al12Mg17,Al3Mg2)转变为Al-Mg固溶体。与400℃相比,450℃时Al/Ta界面扩散层宽度增大。在400℃和450℃时,AZ31/Al/Ta复合材料抗剪强度分别为24 MPa和46 MPa。AZ31/Al/Ta复合材料界面结合机制为扩散与机械啮合共存。此外,避免界面脆性相的形成可以显著提高界面结合强度。

    Abstract:

    The Mg/Ta composite material exhibits both exceptional resistance to high-energy particle irradiation and lightweight characteristics, enabling it to more effectively address the requirements of future deep-space exploration. However, joining these two dissimilar metals is challenging due to their significant differences in properties. In this work, AZ31/Al/Ta composites were successfully prepared using the vacuum hot compression bonding (VHCB) method. The effect of hot compressing temperature on the interface microstructure evolution, phase constitution, and shear strength at the interface was investigated. Moreover, the interface bonding mechanisms of the AZ31/Al/Ta composites under the VHCB process conditions were explored. The results demonstrated that as the VHCB temperature increased, the phase composition of the interface between Mg and Al changed from the Mg-Al brittle IMCs (Al12Mg17, Al3Mg2) to the Al-Mg solid solution. Meanwhile, the width of the Al/Ta interface diffusion layer increased to 450℃ compared to that at 400℃. The shear strengths were 24 MPa and 46 MPa at 400℃ and 450℃, respectively. The interfacial bonding mechanism of AZ31/Al/Ta composites involves the coexistence of diffusion and mechanical meshing. Avoiding the formation of brittle phases at the interface can significantly improve interfacial bonding strength.

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于智磊,李景利,韩修柱,李佰锐,薛志勇.温度对真空热压连接技术制备AZ31/Al/Ta复合材料界面组织和力学性能的影响[J].稀有金属材料与工程,,().[Yu Zhilei, Li Jingli, Han Xiuzhu, Li Bairui, Xue Zhiyong. Effect of Temperature on the Interface Microstructure andMechanical Properties of AZ31/Al/Ta Composites Prepared by Vacuum Hot Compression Bonding[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-09-17
  • 最后修改日期:2024-11-18
  • 录用日期:2024-12-02
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