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喷砂对4777DS高温合金再结晶影响及其机理研究
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1.东方电气集团东方汽轮机有限公司;2.北京科技大学

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清洁高效透平动力装备全国重点实验室开放课题资助(项目号No. DEC8300CG202320365EE280525)


Effect of Sandblasting on Recrystallization Defects of Directional Solidification 4777DS Superalloys
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    摘要:

    采用光学显微镜、扫描电子显微镜研究了不同喷砂工艺对4777DS合金再结晶缺陷的影响以及合金产生再结晶的情况。对喷砂的合金表面再结晶组织分析结果表明,随着喷砂强度增加、时间延长、砾径增加以及喷砂距离的减少,合金表面再结晶的深度增加。经喷砂后的变形试样,接近喷砂表面的γ′相由蝶状变成长条状,部分变形γ′相环绕在变形较大的区域,同时由TEM可观察到在γ基体通道与γ′相中分布着大量位错。枝晶干与枝晶间不同的γ′相会影响再结晶的生长,从而使再结晶晶界形成波浪状形貌,未发现共晶及碳化物对再结晶的抑制作用。由于表层再结晶晶粒较小及残存应力的存在,次表层会形成新一层的再结晶晶粒。

    Abstract:

    Nickel based superalloy 4777DS is used in turbine blades and other engine components due to its creep strength and oxidation resistance at high temperatures. Surface recrystallization can have adverse effects on the mechanical properties of alloys. The effects of different sand-blasting processes on recrystallization defects and the occurrence of recrystallization in 4777DS alloy were studied using optical microscopy and scanning electron microscopy. The analysis of the recrystallization structure on the alloy surface after sandblasting shows that the depth of recrystallization on the alloy surface increases with the increase of sandblasting intensity, time, gravel diameter, and the decrease of sandblasting distance. After sandblasting, the deformed sample showed that the γ "phase near the sandblasted surface changed from a butterfly shape to a long strip shape, and some of the deformed γ" phase surrounded the areas with greater deformation. At the same time, TEM observed a large number of dislocations distributed in the γ matrix channels and γ "phase. The different gamma "phases between dendrites affect the growth of recrystallization, resulting in the formation of wavy grain boundaries. No inhibitory effect of eutectic or carbide on recrystallization has been found. Due to the small size of surface recrystallized grains and the presence of residual stress, a new layer of recrystallized grains will form in the subsurface.

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张琼元,张子越,杨啊涛,姚志浩,贺群功,王海洋,董建新.喷砂对4777DS高温合金再结晶影响及其机理研究[J].稀有金属材料与工程,,().[ZhangQiongYuan, ZhangZiYue, YangATao, YaoZhiHao, HeQunGong, WangHaiYang, DongJianXin. Effect of Sandblasting on Recrystallization Defects of Directional Solidification 4777DS Superalloys[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-11-22
  • 最后修改日期:2025-01-16
  • 录用日期:2025-01-21
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