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枝晶细化对第三代单晶高温合金显微组织和持久性能的影响
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1.深圳市万泽航空科技有限责任公司;2.中南大学 粉末冶金国家重点实验室;3.中南大学

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TG132

基金项目:

深圳市科技计划项目(JSGG20220831092800001)


Effect of dendrite refinement on the microstructure and stress rupture properties of a third-generation single crystal superalloy
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Shenzhen Science and Technology Program(JSGG20220831092800001)

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    摘要:

    采用第三代单晶高温合金WZ30,在不同工艺条件下制备了具有不同枝晶间距的单晶试样,并对其显微组织和持久性能进行了研究和比较。通过改进定向凝固炉加热室与冷却区之间的隔热效果,试样铸件的平均一次枝晶间距从415 μm减小至251 μm,实现了枝晶和共晶组织的显著细化。同时,经枝晶细化后,样品中铸造疏松的体积比从2.29%降低至0.21%。此外,枝晶细化后,样品中枝晶干和枝晶间区域的γ′相均发生细化,尺寸分布更加均匀,形状更加规则。经过后续固溶和时效处理后,枝晶细化试样中获得了尺寸更小、立方度更高的γ′析出相。结果表明,在980 ℃/280 MPa条件下,枝晶细化后样品的持久寿命提高了13.8%。

    Abstract:

    A third-generation single-crystal superalloy WZ30 was used to produce single-crystal samples with varying dendrite spacings under different processing techniques. The microstructures and stress rupture properties were examined and compared. By improving the isolation between heating and cooling zone of the directional solidification furnace, the mean primary dendrite spacing of the sample castings was reduced from 415 μm to 251 μm, leading to a noticeable refinement of dendrite and eutectic structure. At the same time, dendrite refinement can simultaneously decrease the content of casting porosity from 2.29% to 0.21%. Additionally, following dendrite refinement, the γ′ phase in both the dendritic and inter-dendritic regions undergoes refinement, resulting in a more uniform size distribution and a more regular shape. After the subsequent solution and aging treatment, the smaller γ′ precipitates with higher degree of cuboid were obtained in the dendrite-refined samples. As a result, the stress rupture properties at 980 ℃/280 MPa condition was improved by 13.8%.

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赵运兴,王迪,马德新,魏剑辉,程博文,孙洪元,徐维台,黄再旺.枝晶细化对第三代单晶高温合金显微组织和持久性能的影响[J].稀有金属材料与工程,,().[zhaoyunxing, wangdi, madexin, weijianhui, chengbowen, sunhongyuan, xuweitai, huangzaiwang. Effect of dendrite refinement on the microstructure and stress rupture properties of a third-generation single crystal superalloy[J]. Rare Metal Materials and Engineering,,().]
DOI:10.12442/j. issn.1002-185X.20250275

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历史
  • 收稿日期:2025-05-20
  • 最后修改日期:2025-06-11
  • 录用日期:2025-06-27
  • 在线发布日期: 2025-07-28
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