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无压浸渗法制备高体积分数SiC/Al复合材料的研究
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清华大学材料学院 新型陶瓷与精细工艺国家重点实验室,中国钢研科技集团有限公司,中国钢研科技集团有限公司,中国钢研科技集团有限公司,清华大学材料学院 新型陶瓷与精细工艺国家重点实验室,中国钢研科技集团有限公司

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国家科技重大专项资助项目(2013ZX02104)


Study on Pressureless Infiltration Preparation of High SiC/Al CeramicMatrix Composites
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State Key Laboratory of New Ceramics and Fine Processing,Department of Materials Science and Engineering,Tsinghua University,,,,State Key Laboratory of New Ceramics and Fine Processing,Department of Materials Science and Engineering,Tsinghua University,

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    摘要:

    以SiC粉体及铝合金为主要原料,采用无压浸渗工艺制备得到了SiC/Al复合材料。采用X射线衍射仪(XRD), 扫描电镜(SEM)及万能试验机等检测手段对SiC/Al复合材料的物相组成、显微结构及机械性能进行了表征研究。结果表明,铝合金与SiC粉体浸渗完全;制备得到的SiC/Al复合材料显微结构均匀,无明显气孔存在。SiC/Al复合材料的主晶相为SiC, Al,同时含有少量的Si,Mg2Si和MgAl2O4等相。铝合金中添加Mg可以显著提高铝液的浸润性;与7Mg复合材料相比,10Mg复合材料具有更高的致密度与更好的显微结构。复合材料整体上表现出脆性断裂的特征,SiC颗粒以穿晶解理的方式发生脆断。

    Abstract:

    SiC/Al composites were fabricated by pressureless infiltration technique using the silicon carbide powder and aluminum alloy as the starting materials. The phase, microstructure and mechanical properties of the sample were characterized by SEM, XRD and universal testing machine. The results showed that the SiC/Al composite was infiltrated completely by aluminum alloy. The microstructure of the sample was homogeneous. No obvious pores were detected. The major phases of SiC/Al composites were SiC and Al. Othe weak XRD characteristic peaks such as Si, Mg2Si and MgAl2O4 phase were also observed in SiC/Al composites. The soaking property of liquid Al could be enhanced by the addition of Mg into aluminum alloy. Compared with The composites of 7 Mg, the composites of 10 Mg have higher dentity and better structure. Composites showed the characteristics of brittle fracture. SiC particles were destroyed by the way of transcrystalline cleavage.

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刘秋元,王峰,贺智勇,张启富,谢志鹏,王晓波.无压浸渗法制备高体积分数SiC/Al复合材料的研究[J].稀有金属材料与工程,2018,47(S1):315~318.[LIU Qiuyuan, WANG Feng, HE Zhiyong, ZhANG Qifu, XIE Zhipeng, WANG Xiaobo. Study on Pressureless Infiltration Preparation of High SiC/Al CeramicMatrix Composites[J]. Rare Metal Materials and Engineering,2018,47(S1):315~318.]
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  • 收稿日期:2017-07-03
  • 最后修改日期:2018-02-08
  • 录用日期:2018-02-09
  • 在线发布日期: 2018-10-22
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