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TA15钛合金双重热处理工艺及其微观组织演化的EBSD研究
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EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy
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    摘要:

    针对航空航天工业中广泛应用的近a TA15钛合金,开展了不同热处理参数下的双重热处理实验研究。利用背散射电子技术(Electronic backscatter diffraction, EBSD)表征了不同热处理参数下微观组织形貌特征和晶体学取向分布及规律。对比分析了热处理处保温时间对微观组织形貌及取向分布的影响规律。揭示了双重热处理过程中球化的等轴晶粒,条状次生as晶粒及b转变组织的形成演化过程;分析了不同组织间的晶体取向与位置分布关系。研究表明:双重热处理过程中一次保温时间对等轴初生ap形貌及分布等影响较大;热处理过程中球化的等轴晶粒来源于未转变的ap 相;二次保温时间对as形貌、尺寸等具有显著影响;二次保温过程中细条状as表现为先增长再增厚的生长模式;ap与相邻的as晶体学取向关系表现出一定的统计性规律。

    Abstract:

    The study of dual heat treatment with different parameters has been performed on TA15 titanium alloy, which is a typical near a titanium and widely used in aerospace. The Electronic backscatter diffraction (EBSD) technique has been employed to characterize the microstructure and analyze the crystal orientation distribution of those samples subjected to different heat treatment. The effect of the heat holding time on microstructure morphology and orientation distribution was investigated. The formation and evolution of equiaxed primary ap, lamellar second as and transformed bT during the process of dual heat treatment has been revealed. The crystal orientation relationship between the ap and adjacent as has been analyzed. The results indicate that the holding time of stage I has an obvious influence on the morphology and distribution of ap. The equiaxed ap comes from heat treatment stage I as a result of retained primary ap. The holding time of stage II has a significant effect on the size and morphology of as. The mode of first lengthening and then thickening has been observed during the as coarsening process. A certain degree of match has been found between the crystal orientation of ap and adjacent as.

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朱景川,何 东,杨夏炜,刘 勇. TA15钛合金双重热处理工艺及其微观组织演化的EBSD研究[J].稀有金属材料与工程,2013,42(2):382~386.[Zhu Jingchuan, He Dong, Yang Xiawei, Liu Yong. EBSD Study on Dual Heat Treatment and Microstructure Evolution of TA15 Titanium Alloy[J]. Rare Metal Materials and Engineering,2013,42(2):382~386.]
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  • 收稿日期:2012-02-11
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