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纯钨经高压扭转后韧性及热稳定性观察
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同济大学材料科学与工程学院

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国际热核聚变实验堆(ITER)计划


Observations on the ductility and thermostability of tungsten processed from micropowder by improved high-pressure torsion
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Tongji University

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    摘要:

    采用高压扭转法,在440℃对纯钨进行大塑性变形(HPT)。硬度测试表明试样表面纯钨经高压扭转后硬度高达1150HV。差热分析(DSC)结果表明等效应变较小的试样再结晶温度较高(高于1450℃),等效应变较大的试样再结晶温度较低(约800℃)。XRD分析结果表明试样晶格应变达0.35%,晶格常数达0.3177 nm,位错密度达2.4 × 1015 m-2。高压扭转可以使纯钨在低温下实现固结并具有高强度,一定的韧性和热稳定性。

    Abstract:

    Tungsten was subjected to severe plastic deformation at 440°C using high pressure torsion (HPT) with an improved die-set. Microhardness measurements suggest an appreciable ductility level in tungsten after HPT with Vickers microhardness as high as ~1150 HV. Differential scanning calorimetry (DSC) analyses showed that samples that developed less strain had a higher recrystallisation temperature (greater than 1450°C) than samples that developed more strain (~800°C). X-ray diffraction analyses indicate increases in lattice strain of up to 0.35%, lattice parameter up to 0.3177 nm and dislocation density up to 2.4 × 1015 m-2. The current study introduces the improved HPT process as an effective route for the production of ultrahigh strength W with significant ductility and specified thermostability.

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梁辰.纯钨经高压扭转后韧性及热稳定性观察[J].稀有金属材料与工程,2016,45(12):3089~3094.[LiangChen. Observations on the ductility and thermostability of tungsten processed from micropowder by improved high-pressure torsion[J]. Rare Metal Materials and Engineering,2016,45(12):3089~3094.]
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  • 收稿日期:2014-09-07
  • 最后修改日期:2014-11-14
  • 录用日期:2014-12-25
  • 在线发布日期: 2017-02-06
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