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纳米Cr2O3微粒对2024-T4微弧氧化膜结构及耐磨性能的影响
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哈尔滨工业大学,哈尔滨工业大学

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Effect of Nano Cr2O3 Particles on Microstructure and Wear Resistanceof Micro-arc Oxidation Coatings on 2024-T4 Aluminum Alloy
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    摘要:

    摘 要: 在含有不同浓度纳米Cr2O3微粒的硅酸盐体系电解液中对2024-T4铝合金进行微弧氧化处理,使用SEM观察陶瓷膜的表面形貌和截面形貌,使用EDS能谱仪分析膜层中各主要成分沿截面方向的分布,使用XRD分析陶瓷膜的相结构,使用纳米压痕硬度计测量陶瓷膜的硬度,使用粗糙度仪测量陶瓷膜的表面粗糙度,使用摩擦磨损试验机测量陶瓷膜的摩擦系数,使用激光共聚焦显微镜测量磨痕体积,评估磨损率,使用SEM观察磨痕形貌,结果表明:在电解液中加入纳米Cr2O3微粒后,制备的陶瓷膜中出现了Cr2O3相,电解液中纳米Cr2O3微粒浓度达到2.4g/L时,陶瓷膜的硬度最高,摩擦系数最小,磨损率最低,耐磨性最好。

    Abstract:

    Abstract: 2024-T4 aluminum alloy was treated by micro-arc oxidation in the silicate system electrolyte with different concentrations of nano Cr2O3 microparticles. The surface morphology and the cross-section morphology of ceramic coatings were observed by SEM. The distribution of main component of ceramic coatings along the cross-section was analyzed by EDS, and the phase structure of ceramic coatings was analyzed by XRD. The hardness of ceramic coatings was measured by nano indentation hardness tester. The surface roughness of ceramic coatings was measured by roughness meter. The friction coefficient of ceramic coatings was measured by Friction and wear tester. The wear volume of ceramic coatings were measured by laser confocal microscope and the wear rate was evaluated. The morphology of wear tracks was observed by SEM. The results show that the composition of Cr2O3 was discovered in the ceramic coatings after nano Cr2O3 microparticles were added to the electrolyte. The hardness of ceramic coatings is the highest, the friction coefficient of ceramic coatings is the minimum, the wear rate is the lowest, and the wear resistance of ceramic coatings is the best under the condition of concentration of nano Cr2O3 microparticles being 2.4 g/L in the electrolyte.

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李振伟,狄士春.纳米Cr2O3微粒对2024-T4微弧氧化膜结构及耐磨性能的影响[J].稀有金属材料与工程,2017,46(7):2022~2027.[lizhenwei, dishichun. Effect of Nano Cr2O3 Particles on Microstructure and Wear Resistanceof Micro-arc Oxidation Coatings on 2024-T4 Aluminum Alloy[J]. Rare Metal Materials and Engineering,2017,46(7):2022~2027.]
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  • 收稿日期:2015-03-18
  • 最后修改日期:2015-09-29
  • 录用日期:2015-10-13
  • 在线发布日期: 2017-11-14
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