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β相区热变形诱导TiC/Ti复合材料硅化物析出行为
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1.太原理工大学材料科学与工程学院;2.先进金属复合材料成形技术与装备教育部工程研究中心

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山西省重点研发计划项目 (No. 201903D421084 ,201903D121056);山西省自然科学(201801D221141, 201801D121091)


Precipitation behavior of Silicide in TiCp/Ti composites induced by hot deformation during β phase region
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School of Materials Science and Engineering,Taiyuan University of Technology

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    摘要:

    本实验对5vol.%TiCp/近α钛复合材料进行了β相区的热物理模拟试验,研究了复合材料热变形过程中硅化物的析出行为和β相变形机理。变形后的室温组织中主要由片层α相和破碎的TiCp组成,通过透射电子显微镜(TEM)确定组织中存在(Ti,Zr)6Si3型硅化物,尺寸为350-600nm。硅化物的含量随着温度升高和应变速率增加而减少。此外,根据室温α相重构了β母晶粒。TiCp沿β晶界分布,通过提供形核位点和阻碍位错运动,促进了β相动态再结晶过程。热变形过程中的应变积累和TiCp附近形成的高密度位错诱导和促进了硅化物析出。

    Abstract:

    In this experiment, thermal physical simulation experiments were carried out on 5vol.%TiCp/near-α titanium matrix composites to investigate the precipitation behavior of silicides and the deformation mechanism of β phase during β phase region. After deformation, microstructure is mainly composed of lamellar α phase and broken TiCp at room temperature. The existence of (Ti,Zr)6Si3 silicides in the microstructure was confirmed by transmission electron microscopy (TEM),with the grain size of 350-600nm. The numeber of silicides increases with the increasing temperature or decreasing strain rate. In addition, the parent β grains were reconstructed by α phase at room temperature. TiCp was distributed along the β grain boundary, which promoted the dynamic recrystallization of β phase by providing nucleation sites and hindering dislocation movement. The high-density dislocations induced and promoted the precipitation of silicides caused by accumulation of strain and TiCp during hot deformation.

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张长江,嵇祥,孙永刚,张树志,韩建超.β相区热变形诱导TiC/Ti复合材料硅化物析出行为[J].稀有金属材料与工程,2022,51(4):1531~1536.[Zhang Changjiang, Ji Xiang, Sun Yonggang, Zhang Shuzhi, Han Jianchao. Precipitation behavior of Silicide in TiCp/Ti composites induced by hot deformation during β phase region[J]. Rare Metal Materials and Engineering,2022,51(4):1531~1536.]
DOI:10.12442/j. issn.1002-185X.20210350

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  • 收稿日期:2021-04-21
  • 最后修改日期:2021-05-17
  • 录用日期:2021-05-25
  • 在线发布日期: 2022-05-05
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