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晶粒组织对2195铝锂合金应力时效析出行为与性能的影响
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中南大学 材料科学与工程学院

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中图分类号:

TG146.2

基金项目:

轻质高强结构材料重点实验室项目(JCKY201851);国家自然科学(U21B6004)


Effect of Grain Microstructure on Precipitation Behavior and Properties of 2195 Al-Li Alloy under Stress-aging
Author:
Affiliation:

School of Materials Science and Engineering,Central South University

Fund Project:

Project of Key Laboratory of Lightweight and High Strength Structural Materials(JCKY201851);National Natural Science(U21B6004)

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    摘要:

    本文通过恒应力蠕变拉伸、室温拉伸及慢应变速率拉伸应力腐蚀性能测试等试验,结合OM、SEM、TEM及EBSD等组织观察,分析探究变形和细晶两种不同晶粒组织对应力时效处理2195铝锂合金析出行为与性能的影响。结果表明:与细晶组织板材相比,变形组织板材达到峰值硬度的时间由18h缩短至4h,峰值硬度由165.3HV升高到228HV,抗拉强度由584.6MPa提升至641.9MPa。通过计算细晶强化、位错强化及析出相强化对合金强度提高的贡献值,发现变形组织板材力学性能提升主要来源于位错强化的贡献。同时,与细晶组织板材相比,变形组织板材的 ISSRT值由7.6%降低到4.8%,应力腐蚀敏感性降低。变形组织板材的大角度晶界比例由细晶组织板材的64.6%降低至41.1%,晶界析出相分布更为离散,几乎观察不到无沉淀析出带,是获得较为优异抗应力腐蚀性能的主要原因。

    Abstract:

    In this paper, through tests such as constant stress creep tensile, room temperature tensile and slow strain rate tensile stress corrosion performance tests, combined with OM, SEM, TEM and EBSD microstructure observation and analysis to explore the effects of deformation and fine-grained two different grain structures on stress Effects of aging treatment on precipitation behavior and properties of 2195 Al-Li alloy. The results show that compared with the fine-grained sheet, the time for the deformed sheet to reach the peak hardness is shortened from 18h to 4h, the peak hardness is increased from 165.3HV to 228HV, and the tensile strength is increased from 584.6MPa to 641.9MPa. By calculating the contribution values of grain refinement strengthening, dislocation strengthening and precipitation strengthening to the improvement of alloy strength, it is found that the improvement of mechanical properties of deformed sheet is mainly due to the contribution of dislocation strengthening. At the same time, compared with the fine-grained sheet, the ISSRT value of the deformed sheet was reduced from 7.6% to 4.8%, and the stress corrosion susceptibility was reduced. The proportion of large-angle grain boundaries of the deformed sheet is reduced from 64.6% to 41.1% of the fine-grained sheet, the grain boundary precipitation phase distribution is more discrete, and the precipitation-free zone is hardly observed, which is the main reason for obtaining relatively excellent stress corrosion resistance. reason.

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胡恬娇,叶凌英,董宇,王鹏宇.晶粒组织对2195铝锂合金应力时效析出行为与性能的影响[J].稀有金属材料与工程,2023,52(9):3230~3238.[Hu Tianjiao, Ye Lingying, Dong Yu, Wang Pengyu. Effect of Grain Microstructure on Precipitation Behavior and Properties of 2195 Al-Li Alloy under Stress-aging[J]. Rare Metal Materials and Engineering,2023,52(9):3230~3238.]
DOI:10.12442/j. issn.1002-185X.20220746

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  • 收稿日期:2022-09-19
  • 最后修改日期:2022-11-15
  • 录用日期:2022-11-24
  • 在线发布日期: 2023-09-25
  • 出版日期: 2023-09-21