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T6热处理对粉末触变成形技术制备Ti@(Al-Si-Ti)p/A356Al复合材料组织和性能的影响
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兰州理工大学 省部共建有色金属先进加工与再利用国家重点实验室

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国家自然科学基金资助(项目号51564035)


Effect of T6 heat treatment on the microstructure and properties of Ti@(Al-Si-Ti)p/A356Al composites fabricated via powder thixoforming
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State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou University of Technology

Fund Project:

The National Natural Science Foundation of China (General Program, Key Program, Major Research Plan)

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    摘要:

    本文采用粉末触变成形技术制备了由“芯-壳”结构粒子增强的A356Al复合材料,然后通过T6热处理进一步提高该复合材料的综合力学性能。研究结果表明,“芯-壳”结构增强体颗粒不仅能够提高复合材料的抗拉强度、屈服强度(增加率分别为18.0%和32.7%),而且使其(10.8%)具备与基体铝合金(11.3%)相当的塑性。在T6热处理过程中,随时效时间的延长,该复合材料的强度、硬度先增加(1-7h,即欠时效)后减小(9-12h,即过时效),在8h时达到最大值(即峰时效),此时复合材料的抗拉强度、屈服强度和硬度分别为325.4 MPa、254.4 MPa和104.0 HV,比热处理前分别提高了33.7%、74.0%和48.5%;峰时效延伸率为9.4%,与热处理前相比几乎没有下降。即经过T6热处理后,“芯-壳”结构增强体粒子能在提高复合材料强度的同时,最大程度地保留其良好的塑性。最后,通过对时效8h和12h的复合材料基体中析出相的尺寸、密度和类型的分析,对其强化机制进行了讨论。

    Abstract:

    In this work, an A356 Al alloy based composite reinforced by core-shell structured (CS) particulates was prepared by powder thixoforming, and then further improved the comprehensive mechanical properties of the composite by T6 heat treatment. The results show that the CS particulates not only improved the ultimate tensile strength and yield strength of the composite (increased by 18.0% and 32.7%, respectively), but also rendered the composite an excellent elongation of 12% equivalent to that of the A356 alloy (10.8% and 11.3%, respectively). During the T6 heat treatment, the strength and hardness of the composite increased firstly (1-7h, i.e., under-aging) and then decreased (9-12h, i.e., over-aging) with the extension of the aging time, reaching the maximum value at 8h (i.e., peak aging). The ultimate tensile strength, yield strength and hardness of the composite at peak aging were 325.4 MPa, 254.4 MPa and 104.0 HV, respectively, which were 33.7%, 74.0% and 48.5% higher than those without the heat treatment, and the elongation was 9.4%, which was almost no decrease compared with that without heat treatment. In other words, after the T6 heat treatment, the CS particulates can improve the strength of the composite while retaining its good plasticity. Finally, the strengthening mechanisms of the composite are discussed by analyzing the size, density and type of the precipitates in the matrix of the composites aged for 8h and 12h.

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张治国,陈体军,张学拯,王延明. T6热处理对粉末触变成形技术制备Ti@(Al-Si-Ti)p/A356Al复合材料组织和性能的影响[J].稀有金属材料与工程,2024,53(2):520~528.[zhang zhi guo, chen ti jun, zhang xue zheng, wang yan ming. Effect of T6 heat treatment on the microstructure and properties of Ti@(Al-Si-Ti)p/A356Al composites fabricated via powder thixoforming[J]. Rare Metal Materials and Engineering,2024,53(2):520~528.]
DOI:10.12442/j. issn.1002-185X.20230053

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  • 收稿日期:2023-02-03
  • 最后修改日期:2023-03-24
  • 录用日期:2023-04-07
  • 在线发布日期: 2024-02-28
  • 出版日期: 2024-02-23