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电阻焊接技术制备Nb3Sn-NbTi 混合超导接头
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1.中国科学院电工研究所,北京 100190;2.中国科学院大学,北京 100049;3.齐鲁中科电工先进电磁驱动技术研究院,山东 济南 250102;4.西部超导材料科技股份有限公司,陕西 西安 710018

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Preparation of Nb3Sn-NbTi Hybrid Superconducting Joint by Resistive Welding Technique
Author:
Affiliation:

1.Institute of Electrical Engineering, Chinese Academy of Sciences, Beijing 100190, China;2.University of Chinese Academy of Sciences, Beijing 100049, China;3.Institute of Electrical Engineering and Advanced Electromagnetic Drive Technology, Jinan 250102, China;4.Western Superconducting Technologies Co., Ltd, Xi 'an 710018, China

Fund Project:

National Key R&D Program of China (2022YFB3804004, 2022YFF0706904); National Natural Science Foundation of China (52307032)

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    摘要:

    在强磁场超导磁体应用中,特别是具有高稳定度高场超导磁体,具有极低电阻的超导接头发挥着重要作用。通过电阻焊接方法制备了Nb3Sn 和NbTi的异种材料超导接头。首先通过烧结法制备了Nb3Sn的超导接头,然后通过电阻焊接将Nb3Sn超导接头与NbTi超导体焊接成型。分析了Nb3Sn超导接头制备过程中Nb3Sn的微观组织结构和相变。利用无损检测CT对接头结构进行三维重构,分析了Nb3Sn 和NbTi超导接头内部的缺陷和2种不同材料间的微观连接状态。最后,在背景磁场下对超导接头的电阻性能进行了测试和研究。结果表明,与传统超导焊料制备的超导接头相比,电阻焊接制备的超导接头显示出良好的耐磁场性能,在1.5 T背景磁场下具有较低的电阻值。

    Abstract:

    In high magnetic field magnets, especially those with high stability requirements, superconducting joints with ultra-low resistances play an important role in magnet fabrication. The Nb3Sn and NbTi joints were fabricated by the resistive welding technique. The Nb3Sn joint was fabricated by sintering the Nb-Sn precursors after mechanical alloying. Then the Nb3Sn bulk in the Nb3Sn joint was welded to the NbTi conductor. The microstructure and grain sizes of Nb3Sn bulk after long periods of time at high temperature were investigated. After welding, the joint was analyzed using X-ray nano-CT technology to display the connecting status and the defects between the Nb3Sn and NbTi conductor without destroying the joint. The electrical characteristics of the joints were measured under background fields through the field decay method. Results show that compared with the ones prepared by the commonly used solid matrix replacement technique, the prepared joint exhibits better magnetic field resistance and lower resistance at 1.5 T background field.

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孙万硕,程军胜,王磊,陈顺中,郭强.电阻焊接技术制备Nb3Sn-NbTi 混合超导接头[J].稀有金属材料与工程,2023,52(12):4040~4046.[Sun Wanshuo, Cheng Junsheng, Wang Lei, Chen Shunzhong, Guo Qiang. Preparation of Nb3Sn-NbTi Hybrid Superconducting Joint by Resistive Welding Technique[J]. Rare Metal Materials and Engineering,2023,52(12):4040~4046.]
DOI:10.12442/j. issn.1002-185X.20230493

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历史
  • 收稿日期:2023-08-08
  • 最后修改日期:2023-09-25
  • 录用日期:2023-10-07
  • 在线发布日期: 2023-12-25
  • 出版日期: 2023-12-22