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显微组织对FGH4113A高温合金热变形行为和组织演变的影响
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1.深圳市万泽航空科技有限责任公司;2.深圳市万泽中南研究院有限公司;3.中南大学 粉末冶金国家重点实验室;4.Powder Metallurgy Research Institute, Central South University

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深圳市科技计划资助 KJZD20230923113900001


Influence of Initial Microstructures on the Hot Deformation Behavior and Microstructure Evolution of FGH4113A Superalloy
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Affiliation:

1.Shenzhen Wedge Aviation Technology Co., Ltd;2.Shenzhen Wedge Central South Research Institute Co., Ltd;3.Powder Metallurgy Research Institute, Central South University;4.中南大学 粉末冶金国家重点实验室

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Shenzhen Science and Technology Program KJZD20230923113900001

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    摘要:

    为理解粉末高温合金FGH4113A的热变形性能,采用热压缩试验研究不同初始显微组织对其热变形行为和显微组织演变过程的影响。三种状态分别是:热等静压态(A1)、热等静压+1100℃挤压(A2)、热等静压+1500℃挤压(A3)。结果表明:1100℃挤压的A2样品具有均匀的γ+γ′双相细晶粒组织,1050℃和1100℃均表现出良好的热变形性能。在较大应变范围内,A2样品的真应力-真应变曲线保持了硬化-软化平衡状态,变形后平均晶粒尺寸5μm。热等静压态A1样品和1150℃挤压A3样品1050℃仍处于变形软化阶段,组织为原始粗大晶粒和细小再结晶晶粒的混合项链晶,样品的再结晶形核机制主要为应变诱发晶界弓弯形核。1150℃-0.001s-1时,初始组织对热压缩变形和变形后组织影响不明显,变形后组织为粗大的再结晶晶粒。细晶组织有利于提高合金的变形性能,通过合理的热变形制度,可以获得均匀细小的显微组织。

    Abstract:

    To fully harness the hot deformation capabilities of the FGH4113A superalloy and ascertain the influence of different initial microstructures on its hot deformation behavior and microstructural evolution, the hot compression curves and deformed microstructures were investigated under various hot deformation conditions for FGH4113A superalloy in three states: Hot Isostatic Pressing (HIP, as A1), HIP+ Hot extruded at 1100℃(A2), and HIP+ Hot extruded at 1150℃(A3). The results show that A2, extruded at 1100℃ with uniformly γ+γ′ microduplex microstructures, demonstrated commendable hot deformation behavior at both 1050℃ and 1100℃. The true stress-strain curves of A2 maintained a prolonged hardening-softening equilibrium over an extended strain range, with post-deformation average grain sizes being within 5μm. On the other hand, the HIP-conditioned A1 and the 1150℃ extruded A3 exhibited a softening region in deformation curves at 1050℃, and the grain microstructures reflect an incomplete recrystallized state—a blend of fine recrystallized grains and the initial larger grains, forming a necklace-like microstructure. The predominant recrystallization mechanism for these samples was identified as strain-induced boundary migration. At 1150℃ with a strain rate of 0.001s-1, the impact of the initial microstructure on hot deformation behavior and resultant microstructure was relatively subtle, with post-deformation microstructures predominantly showcasing large, fully recrystallized grains. Fine-grained microstructures are conducive to maximizing the alloy"s hot deformation potential. By judiciously managing deformation regimes, a fine and uniform deformed microstructure can be obtained.

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杨金龙,尹超,熊江英,程俊义,郭建政,冯赣江.显微组织对FGH4113A高温合金热变形行为和组织演变的影响[J].稀有金属材料与工程,,().[yangjinlong, Yin Chao, Xiong Jiangying, Cheng Junyi, Guo Jianzheng, Feng Ganjiang. Influence of Initial Microstructures on the Hot Deformation Behavior and Microstructure Evolution of FGH4113A Superalloy[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-04-03
  • 最后修改日期:2024-06-18
  • 录用日期:2024-07-08
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