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亚稳β-Ti-1023合金不均匀变形行为及应变速率敏感性研究
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1.中北大学 材料科学与工程学院;2.西北工业大学 材料学院

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山西省高等学校科技创新项目(2023L169); 山西省引进科研博士科研启动经费(110136019); 晋财教[2023]第一批优秀博士科研启动经费(9800192)


Investigation on the heterogeneous deformation behavior and strain rate sensitivity of the metastable β-Ti-1023 alloy
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    摘要:

    本文采用数字图像相关技术(Digital image correlation, DIC)实时追踪不同应变速率下应变分布及局部应变演变规律,研究应变分布的传播行为及其应变速率敏感性;采用背散射电子衍射技术(Electron backscatter diffraction, EBSD)技术分析材料变形后微观组织演化及应力诱导马氏体转变(stress induced martensite transformation, SIMT)和马氏体孪晶的演变过程;采用扫描电子显微镜(Scanning electron microscope, SEM)技术观察分析材料的断口形貌。可以得出以下结论:(1) 应变分布由近似于均匀分布向非均匀分布演变,呈现出了应变集中现象,最终在应变集中区域发生断裂,且低应变速率下试样的颈缩现象最明显;(2) 应力-应变曲线呈现明显的双屈服现象,表现出负应变速率敏感性效应,即低应变速率可以产生更高的应变硬化率;(3) 随着应变速率降低,马氏体含量显著增加,晶粒尺寸明显细化,内核平均取向差(Kernel average misorientation,KAM)和几何必须位错(Geometrically necessary dislocations,GNDs)平均值显著增大,说明SIMT含量增加有助于变形试样的位错密度累积,更有利于多种塑性变形机制的耦合作用;(4) 断口形貌呈拉伸型,主要由韧窝型空洞聚合造成。变形过程中韧窝受力从单向受拉迅速向三向受拉发展,韧窝得到充分长大,低应变速率变形促进此特征发生,所以韧性断裂特征占优。

    Abstract:

    The digital image correlation (DIC) technology has been used to track promptly the strain distribution and local strain evolution under different strain rates in this paper, and the propagation behavior of strain distribution and its strain rate sensitivity have been investigated. And the electron backscatter diffraction (EBSD) has been selected to analyze the microstructure evolution, the distribution of stress induced α" martensite transformation (SIMT) and martensite twinning after deformation. Besides, the scanning electron microscope (SEM) has been adopted to observe the fracture morphology of the material. The following conclusions can be drawn: (1) The strain distribution evolved from an approximate uniform distribution to a non-uniform distribution, then showing a phenomenon of strain concentration, and ultimately occurring fracture in the strain concentration area, and the significanted necking phenomenon has been displayed at the low strain rates. (2) A clear double yield phenomenon has been exhibited in the stress-strain curves with producing higher strain hardening rates at the low strain rates, it means that the materials show a negative strain rate sensitivity effect. (3) The content of α" martensite increased significantly, the grain size refined obviously, and the average values of KAM (Kernel average misorientation) and GNDs (Geometrically necessary dislocations) increased dramatically with the strain rate decreasing, it indicates that the SIMT increase can contribute to the accumulation of dislocation density in the deformed sample and be more conducive to the coupling effect of multiple plastic deformation mechanisms. (4) The fracture morphology mainly occur tensile fracture by the aggregation of ductile dimples and voids. The stress on the dimples rapidly develops from unidirectional tension to triaxial tension resulting in sufficient growth of the dimples during the deformation process. Therefore, the ductile fracture characteristics dominated in the low strain rates deformation with promoting the occurrence of this phenomenon.

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王雪丽,李付国,贾鹏来,张治民,王强.亚稳β-Ti-1023合金不均匀变形行为及应变速率敏感性研究[J].稀有金属材料与工程,,().[wangxueli, lifuguo, jiapenglai, zhangzhimin, wangqiang. Investigation on the heterogeneous deformation behavior and strain rate sensitivity of the metastable β-Ti-1023 alloy[J]. Rare Metal Materials and Engineering,,().]
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  • 收稿日期:2024-09-03
  • 最后修改日期:2024-10-29
  • 录用日期:2024-11-08
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