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AlN陶瓷与Al低温钎焊钎料设计及接头组织性能研究
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1.哈工大郑州研究院;2.哈尔滨工业大学 材料结构精密焊接与连接全国重点实验室;3.河南省科学院材料研究所;4..哈工大郑州研究院;5.格力电器(郑州)有限公司;6.卧龙电气南阳防爆集团股份有限公司

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国家自然科学基金项目(面上项目,重点项目,重大项目),中国博士后科学基金


Design of brazing material and study on joint microstructure and properties for low-temperature brazing of AlN ceramics and Al
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The National Natural Science Foundation of China (General Program, Key Program, Major Research Plan),China Postdoctoral Science Foundation

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    摘要:

    本研究针对目前缺乏适合AlN陶瓷和Al低温钎焊的钎料的问题,通过向AgCuTi钎料中加入In和Sn元素,来降低钎料熔点,制备了新型低温钎料AgCu28In35Ti2和Sn48.15Ag19Cu14.35In 17.5Ti1,从而实现AlN/Al接头的良好连接。探究了两种钎料对AlN陶瓷和Al的低温钎焊工艺和接头组织形貌及性能。研究表明:SnAgCuInTi钎料在钎缝处形成了InSn3,Al3Ti等相对稳定的化合物。AgCuInTi钎料在钎缝处生成Al2Cu、AgIn2和TiAl3等相对稳定的化合物,随着焊接温度的增加,接头强度随之提高。为阻止In的扩散析出,选择在Al表面镀Ni,但镀Ni使接头导热性能有所下降。发现使用AgCu28In35Ti2钎料进行焊接,在640℃30min的条件下,接头强度最高,为20.28MPa;在620℃15min的条件下,热扩散系数可达到65.941 m2/s。该钎料为AlN陶瓷/Al的高可靠连接提供了一种新的方法。

    Abstract:

    This study addresses the current lack of brazing materials suitable for low-temperature brazing of AlN ceramics and Al. By adding In and Sn elements to AgCuTi brazing materials to lower their melting points, new low-temperature brazing materials AgCu28In35Ti2 and Sn48.15Ag19Cu14.35In17.5Ti1 were prepared to achieve good bonding of AlN/Al joints. Explored the low-temperature brazing process, joint microstructure and properties of AlN ceramics and Al using two types of brazing materials. Research has shown that SnAgCuInTi brazing materials form relatively stable compounds such as InSn3 and Al3Ti at the solder joints. AgCuInTi brazing material generates relatively stable compounds such as Al2Cu, AgIn2, and TiAl3 at the solder joint, and the joint strength increases with the increase of welding temperature. To prevent the diffusion and precipitation of In, Ni plating was chosen on the surface of Al, but Ni plating reduced the thermal conductivity of the joint. It was found that using AgCu28In35Ti2 brazing material for welding resulted in the highest joint strength of 20.28MPa at 640 ℃ for 30 minutes; Under the condition of 620 ℃ for 15 minutes, the thermal diffusion coefficient can reach 65.941 m2/s. This brazing material provides a new method for highly reliable connection of AlN ceramics/Al.

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周航泽,龙飞,徐瑞,王策,何鹏,施清清,赵岩. AlN陶瓷与Al低温钎焊钎料设计及接头组织性能研究[J].稀有金属材料与工程,,().[Zhou Hangze, Long Fei, Xu Rui, Wang Ce, He Peng, Shi Qingqing, Zhao Yan. Design of brazing material and study on joint microstructure and properties for low-temperature brazing of AlN ceramics and Al[J]. Rare Metal Materials and Engineering,,().]
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历史
  • 收稿日期:2024-09-28
  • 最后修改日期:2024-12-18
  • 录用日期:2024-12-19
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