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ZrO2(ZrB2)活性扩散障界面演变行为的研究
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西安建筑科技大学,西北有色金属研究院,西安建筑科技大学,西北有色金属研究院

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TG174.44

基金项目:

国家重点基础研究发展计划(973计划)2012CB625102; 西安建筑科技大学博士生创新基金(6040300566)


The studies on the interfacial evolution behavior of ZrO2(ZrB2) active diffusion barrier
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School of Metallurgical Engineering,Xi’an University of Architecture and Technology,Xi’an,Northwest Institute for Nonferrous Metal Research,School of Metallurgical Engineering,Xi’an University of Architecture and Technology,Xi’an,Northwest Institute for Nonferrous Metal Research,Xi’an

Fund Project:

The National Basic Research Program of China (973 program 2012CB625102); 2015 Doctoral Innovation Fund at Xi’an University of Architecture and Technology.( 6040300566)

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    摘要:

    本实验采用电子束物理气相沉积(Electron Beam Physical Vapor Deposition, EB-PVD)技术在镍基单晶合金Rene N5基体上制备出N5/(ZrB2+ZrO2)/ NiCrAl和N5/ZrO2/ NiCrAl两组试样。然后,同时对其进行900℃/5h恒温氧化和1000℃/250h、1000℃/300h及1000℃/350h循环氧化,并采用SEM、EDS分析方法研究了界面演变行为及退化失效行为,结果表明,ZrB2的加入对活性扩散障界面反应的生成速率有一定的延缓,但不影响具有阻扩散功能的Al2O3扩散障层的最终形成;并且,ZrB2的加入提高了活性扩散障结构的服役寿命,改变了活性扩散障结构的失效方式。

    Abstract:

    In this paper, two sample groups, N5/(ZrB2+ZrO2)/NiCrAl and N5/ZrO2/NiCrAl, were prepared on Ni-based single crystal alloy (Rene N5) substrate by electron beam physical vapor deposition (EB-PVD). Both sample groups were exposed to isothermal oxidation at 900 °C for 5 h and at 1000 °C, for 250 h, 300 h or 350 h. The microstructural evolution and deterioration failure behavior was investigated by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The results suggest that the introduction of ZrB2 decelerates the interfacial reaction rate of the active diffusion barrier of Al2O3 but did not affect the final formation of the Al2O3 diffusion barrier with anti-diffusion properties. Moreover, the introduction of ZrB2 prolongs the service life of active diffusion barrier structure and changes its failure mode.

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刘林涛,李争显,杨晨曦,何飞. ZrO2(ZrB2)活性扩散障界面演变行为的研究[J].稀有金属材料与工程,2018,47(5):1365~1369.[Lintao Liu, Zhengxian Li, Chenxi Yang, Fei He. The studies on the interfacial evolution behavior of ZrO2(ZrB2) active diffusion barrier[J]. Rare Metal Materials and Engineering,2018,47(5):1365~1369.]
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  • 收稿日期:2016-09-05
  • 最后修改日期:2016-11-14
  • 录用日期:2016-12-02
  • 在线发布日期: 2018-06-08
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