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退火温度对TC18钛合金组织及织构演变规律的影响
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北京航空材料研究院,北京航空材料研究院,北京科技大学材料科学与工程学院,北京航空材料研究院,北京航空材料研究院

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国家自然科学基金资助项目(59493300);教育部博士点基金资助项目(9800462)


Effect of Annealing Temperature on Microstructure and Texture Evolution of TC18 Titanium Alloy
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Beijing Institute of Aeronautical Materials,Beijing Institute of Aeronautical Materials,School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing Institute of Aeronautical Materials,Beijing Institute of Aeronautical Materials

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    摘要:

    随着钛合金锻件的大型化,锻造过程中应力场、温度场不均匀问题更加突出,锻件局部形成锋锐织构的可能性大大增加,易对产品的可靠性及安全性造成危害。本文利用EBSD技术,对比了工业生产的大规格TC18钛合金棒材不同位置中心及表层的组织及织构差异,通过观察两者在不同保温温度下α相及β相的组织及织构特征,研究退火后组织及织构演变规律。结果表明:在两相区,β相主要发生回复,部分α相发生再结晶,β相晶粒尺寸及织构基本不发生变化。接近相变点时,大尺寸回复态β晶粒易于利用尺寸优势吞并其他晶粒;部分α相,特别是晶界处取向接近的片层α相,易于通过合并发生晶粒长大;特殊取向的α相更易发生相变,相变的α相不会形成新的β晶核。在单相区,β相发生再结晶及晶粒长大,且无择尤现象,β相织构明显减弱。

    Abstract:

    Sharp texture in large sizing integration of titanium alloy forgings, which were more easily formed by heterogeneity of stress field and temperature field during forging, is harmful for safety and reliability of products application. By use of EBSD techniques this paper observed the microstructure and texture of TC18 titanium bars at center layer and surface layer, and analyzed the evolution regularity of microstructure and texture after forging and annealing process under different temperature. Results show that after α+β region annealing, most β grains were recovered, some α grains recrystallized, and the grains size and texture of β phases were scarcely changed. When annealed near phase transformation temperature, large sized recovery β grains grew by grains size advantage; some α grains, particularly the lamellar α grains in β grain boundaries, grew by the combination of near oriented α grains; some special oriented α grains trended to transform, the transformed α grains would not create new β phase nuclei. After β region annealing, β phase texture were weakened obviously because β grains recrystallized and grew up without orientation preference.

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颜孟奇,沙爱学,李凯,张旺峰,王玉会.退火温度对TC18钛合金组织及织构演变规律的影响[J].稀有金属材料与工程,2017,46(S1):156~160.[Yan Mengqi, Sha Aixue, Li Kai, Zhang Wangfeng, Wang Yuhui. Effect of Annealing Temperature on Microstructure and Texture Evolution of TC18 Titanium Alloy[J]. Rare Metal Materials and Engineering,2017,46(S1):156~160.]
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  • 收稿日期:2016-05-12
  • 最后修改日期:2016-05-12
  • 录用日期:2017-08-08
  • 在线发布日期: 2017-12-13
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