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Effects of homogenization treatment on the microstructures of 5052-Er Al alloy
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College of Materials Science and Engineering,Chongqing University,Chongqing,400044,College of Materials Science and Engineering,Chongqing University,Chongqing,400044,College of Materials Science and Engineering,Chongqing University,Chongqing,400044,College of Materials Science and Engineering,Chongqing University,Chongqing,400044

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    Abstract:

    The effects of single-step, two-step and three-step homogenization treatments on the microstructures of 5052-Er Al alloy were studied by optical microscopy, scanning electron microscopy and transmission electron microscopy. The results showed that after 560℃/30h high temperature homogenization treatment, most of the non-equilibrium eutectic phases existed in the as-cast alloy dissolved, with the remaining phases being Fe-rich phases like Al3Fe and Al-Fe-Er. The second step treatment performing at lower temperature was found to be beneficial to the spherization and refinement of the Fe-rich phases. The results also showed that homogenization treatment regimes had an obvious effect on the precipitation behavior of the fine precipitates. During the slow cooling process from 560℃/30h isothermally holding to room temperature, there were a large amount of rod β’(Al3Mg2) and spherical Al3(Er, Zr) and Al3Zr phases precipitating out of the matrix. The total volume fraction of the precipitates, 7.4%, was the highest among the four regimes conducted in this experiment. However, these precipitates distributed unevenly and their sizes differed greatly with each other. The second step treatment favored the formation of fine and homogenously distributed precipitates of Al3(Er, Zr) and Al3Zr. When the second step treatment was carried out at 150℃, the quantity density of the precipitates was the highest (20.3um-1) with the finest particle size(average radius being 14nm). Three-step homogenization treatment could obtain a higher quantity density while maintaining a comparable particle size with that in two-step treatment.

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[Zhang Jing, Tang Cong, Zhao Jingjing, Zuo Rulin. Effects of homogenization treatment on the microstructures of 5052-Er Al alloy[J]. Rare Metal Materials and Engineering,2017,46(11):3491~3497.]
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History
  • Received:August 18,2015
  • Revised:November 11,2015
  • Adopted:December 08,2015
  • Online: December 13,2017
  • Published: