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The influence of sputtering power and gas pressure on the preparation of tungsten films by DC magnetron sputtering
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1.School of Materials Science and Engineering,Beijing Institute of Technology

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    Abstract:

    Tungsten films have excellent characteristics such as high melting point, high conductivity,stable chemical properties, and strong radiation resistance, and are widely used in microelectronics, nuclear energy engineering and other fields. Since the structure and performance of the film have a strong dependence on the deposition parameters, it is essential to control the process parameters of the deposition process to obtain a tungsten film with excellent properties. This paper studies the effects of sputtering power and sputtering pressure on the deposition rate, microstructure, and phase structure of tungsten films. Using DC magnetron sputtering technology, a tungsten film is prepared on a Si substrate at room temperature. Atomic force microscope, XRD, four-probe resistance measurement, profiler, etc. were used to characterize the structure and electrical properties of the film. The results show that the deposition rate of the film is affected by the sputtering power and the gas pressure. The deposition rate increases linearly with the increase of the power, and first increases to a peak and then decreases with the increase of the gas pressure. The resistivity and surface roughness of the film depend on the sputtering pressure, and increase with the increase of the sputtering pressure. The increase in the resistivity of the film may be caused by the increase in the surface roughness. Under constant sputtering power, the formation of α-W mainly depends on the sputtering gas pressure. All β-W phases are formed under high pressure, but for the sputtering power is large enough, under higher pressure, the formation of some α-W phases will also be observed. The formation of the specific phase structure (α-W/β-W) in the tungsten film is not only dependent on the deposition pressure, but also related to the sputtering power, which may be related to the energy of the atoms incident on the substrate.

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[Xing Xiaoshuai, Liu Yingxia, Yu Xiaodong, Zhao Xiuchen, Nie Zhihua, Tan Chengwen. The influence of sputtering power and gas pressure on the preparation of tungsten films by DC magnetron sputtering[J]. Rare Metal Materials and Engineering,2022,51(2):682~688.]
DOI:10.12442/j. issn.1002-185X.20210135

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History
  • Received:February 19,2021
  • Revised:March 25,2021
  • Adopted:April 16,2021
  • Online: March 09,2022
  • Published: February 28,2022