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Microstructure and mechanical properties of Ti(N)-TiBw composites prepared in situ by Ti-BN powder metallurgy
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Zhejiang Provincial Natural Science Foundation of China

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    Abstract:

    In this paper, Ti(N)-TiBw composites were prepared by spark plasma sintering (SPS) with pure Ti powder and BN powder as raw materials. The effect of annealing temperature on microstructure evolution and mechanical properties of Ti(N)-TiBw composites was studied. Results show that Ti and BN react in situ to form dense TiBw and N solution strengthened titanium matrix composites when sintered at 1000 ℃. TiBw is distributed in the primary particle boundary in the form of needle like network. With the increase of heat treatment temperature, the aspect ratio of TiBw first increases and then decreases, reaching the maximum at 1100 ℃. However, when the annealing temperature is above 1100 ℃, TiBw coarsens gradually, and the microstructure changes from needle shape to short rod shape. The pinning effect of TiBw on the matrix is obviously weakened, and the grain size of Ti matrix coarsens gradually. The morphology evolution of TiBw follows Ostwald ripening mechanism. As the heat treatment temperature increases, the ultimate tensile strength of the composites first increases and then decreases, reaching a maximum value of 908 MPa at 1000 ℃. The strength improvement is attributed to grain refinement, TiBw load transfer and O/N solution strengthening.

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[cheyan, li shufeng, nan yingying, zhou shengyin, yang shenghui. Microstructure and mechanical properties of Ti(N)-TiBw composites prepared in situ by Ti-BN powder metallurgy[J]. Rare Metal Materials and Engineering,2022,51(8):2933~2941.]
DOI:10.12442/j. issn.1002-185X.20210585

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History
  • Received:July 06,2021
  • Revised:July 20,2021
  • Adopted:August 12,2021
  • Online: September 05,2022
  • Published: August 29,2022