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Microstructure and Properties of 93W-4.6Ni-2.4Fe Prepared by Ball-Milling and Liquid Phase Sintering
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1.School of Materials Science and Engineering, Tianjin University, Tianjin 300072, China;2.ATTL Advanced Materials Co., Ltd, Beijing 100094, China;3.Haitian Plastics Machinery Group Co., Ltd, Ningbo 315801, China

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Fund Project:

National Key R&D Program of China (2023YFB3712002); National Natural Science Foundation of China (U22A20172, 52171044)

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    Abstract:

    In order to produce economical tungsten alloys with superior mechanical properties, 93W-4.6Ni-2.4Fe (wt%) tungsten heavy alloys were fabricated by ball milling and liquid phase sintering at a temperature range of 1450?1510 °C. The microstructure and the fracture modes of the specimens were examined. Results show that the specimens sintered at different temperatures display similar dual-phase microstructure and ductile fracture modes. With the increase in sintering temperature, the tungsten particle size also gradually grows. At the temperatures above 1480 °C, the relative density reaches above 99.0%. The optimal sintering temperature of the specimen with the best tensile strength (940 MPa) and elongation (32.6%) combination is determined to be 1480 °C. The excellent ductility of the specimen sintered at 1480 °C is associated with the network structure of γ phase, the uniform distribution of dimples and the synergistic effect of these two phases. The high strength of the specimen is attributed to the refined tungsten particle size and the spherical tungsten particles.

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[Wang Zitong, Dong Di, Xiong Ning, Xu Jiawei, Dong Zhi, Ma Zongqing. Microstructure and Properties of 93W-4.6Ni-2.4Fe Prepared by Ball-Milling and Liquid Phase Sintering[J]. Rare Metal Materials and Engineering,2024,53(5):1229~1235.]
DOI:10.12442/j. issn.1002-185X.20230778

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History
  • Received:December 01,2023
  • Revised:February 19,2024
  • Adopted:February 26,2024
  • Online: May 27,2024
  • Published: May 22,2024