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In situ synthesis of Ti4AlN3 reinforced with Al2O3 particles by hot isostatic pressing
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Shenyang University of Technology, Shenyang, 110870,,

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    Abstract:

    Bulk intermetallic-ceramic composite Al2O3/Ti4AlN3 was fabricated by in-situ hot isostatic pressing of Al3Ti/TiN nanopowders under 1280 ℃/150 MPa/1 h conditions . The microstructure of composite were investigated by X-ray diffraction, SEM(Scanning Electron Microscope) and TEM(Transmission Electron Microscope). It is revealed that matrix Ti4AlN3 grains are strip-like and Al2O3 particles disperse in matrix uniformly with irregular shape. The averagegrain size of Ti4AlN3 is 7 μm. The size of Al2O3 particles are in the range of 1-3 μm, and volume fraction is about 40%. The Vickers hardness of Al2O3/Ti4AlN3 composite is 6.7GPa, maximal compressed strength is 1 800 MPa. Maximum compressive strain increased from 4% to 6.2%.Compared with the micro-hardness and compressed strength,Al2O3/Ti4AlN3 composite is higher than single Ti4AlN3 phase. The strengthening mechanisms of composite are fine grain strengthening and second phase strengthening.

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[zhengzhuo, sunweimin, liuzheng. In situ synthesis of Ti4AlN3 reinforced with Al2O3 particles by hot isostatic pressing[J]. Rare Metal Materials and Engineering,2016,45(7):1811~1815.]
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History
  • Received:June 21,2013
  • Revised:March 16,2016
  • Adopted:March 29,2016
  • Online: October 09,2016
  • Published: