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Effect of SPS Cyclic Heat-Treatment on the Microstructure and Properties of 93W-4.9Ni-2.1Fe Alloy
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National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials,South China University of Technology,National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials,South China University of Technology,National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials,South China University of Technology,National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials,South China University of Technology,National Engineering Research Center of Near-Net-Shape Forming for Metallic Materials,South China University of Technology

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TF124

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    Abstract:

    The effect of vacuum cyclic heat-treatment based on spark plasma sintering (SPS) technique on the microstructure, composition and properties of as-sintered 93W-4.9Ni-2.1Fe tungsten heavy alloy has been studied by optical microscope, SEM, EDS and three-point bending tests. The results show that the matrix penetration into W-W grain boundaries enhances significantly, and the W-W contiguity and dihedral angle decrease gradually with the cycle index increasing. SPS cyclic heat-treatment does not obviously change the micro-hardness and grain size. The matrix is strengthened by the increasing content of tungsten owing to the treatment. The bending strength of the alloy increases significantly after 2 cycles. When the cycles goes up to 20, the average bending strength reaches 2321MPa, which is 160MPa higher than that of the conventional liquid-sintered and solution-treated 93W-4.9Ni-2.1Fe alloy. The microstructure and properties of 93W-4.9Ni-2.1Fe tungsten heavy alloy can be improved apparently by SPS cyclic heat-treatment.

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[Guan Mo, Li Xiaoqiang, Hu Ke, Yang Fan, Zhu Dezhi. Effect of SPS Cyclic Heat-Treatment on the Microstructure and Properties of 93W-4.9Ni-2.1Fe Alloy[J]. Rare Metal Materials and Engineering,2018,47(7):2210~2215.]
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History
  • Received:July 15,2016
  • Revised:September 30,2016
  • Adopted:November 10,2016
  • Online: October 10,2018
  • Published: