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冯军,陈美艳,童洪辉,金凡亚,但敏,许泽金,沈丽如,张桂凯.低温等离子复合技术制备氧化铝阻氚涂层的研究[J].稀有金属材料与工程(英文),2017,46(10):2837~2841.[fengjun,chenmeiyan,tonghonghui,jinfanya,danmin,xuzejin,shenliru,zhangguikai.Preparation of Alumina Coatings as TritiumPermeation Barrier by a composite Treatment of low temperature plasma[J].Rare Metal Materials and Engineering,2017,46(10):2837~2841.]
Preparation of Alumina Coatings as TritiumPermeation Barrier by a composite Treatment of low temperature plasma
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Received:August 02, 2016  Revised:October 07, 2016
Key words: alumina coatings  tritium permeation barrier  magnetron sputtering  O ion implantation  heat treatment
Foundation item:国家自然科学基金项目(面上项目,重点项目,重大项目)
Author NameAffiliationE-mail
fengjun 南华大学 speedfjkang@163.com 
chenmeiyan 核工业西南物理研究院  
tonghonghui 核工业西南物理研究院  
jinfanya 核工业西南物理研究院  
danmin 核工业西南物理研究院  
xuzejin 核工业西南物理研究院  
shenliru 核工业西南物理研究院  
zhangguikai 中国工程物理研究院
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      In this study, the alumina coatings as tritium permeation barrier were successfully prepared on stainless steel bulk by composite low temperature plasma method of magnetron sputtering, heat treatment and O ion implantation. The phases, surface morphologies, chemical composition and O distribution of the coatings were characterized by XRD, SEM, EDS and AES individually,and after analyzing through scratch adhesion test, thermal shock resistance test and tritium permeability test. The results show that the Al coatings deposited by magnetron sputtering is well, and Fe-Al alloys interlayer was formed after heat treatment. In O ion implantation process, the oxygen depth deepened and the oxygen density gradient decreased with higher accelerating voltage at definite doses, meanwhile it can be seen that 8×1017 ions/cm2 is the crucial dose, above which ion implantation the oxygen density was more homogeneous. After a series tests, the obtained coatings has the good performance with film-substrate cohesion, thermal shock resistance and the tritium permeation resistance, and the coatings, which were treated by superposition at 8×1017 ions/cm2doses, have the best tritium permeability resistance, and it was improved 3 orders of magnitude high than the stainless steel bulk.