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Effect of Tungsten Carbide on Densification and Mechanical Properties of Silicon Nitride Ceramics by Spark Plasma Sintering
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State Key Laboratory of New Ceramics and Fine Processing,Tsinghua University,Liaoning High Temperature Materials and Magnesium Resource Engineering College,University of Science and Technology,Liaoning High Temperature Materials and Magnesium Resource Engineering College,University of Science and Technology,State Key Laboratory of New Ceramics and Fine Processing,Tsinghua University

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    Abstract:

    The high-performance silicon nitride ceramics were prepared by spark plasma sintering (SPS) with Al2O3–Y2O3 as a sintering aid.A novel approch was adopted to fabricate the silicon nitride by introducting WC via mechanical ball milling.The effects of tungsten carbide on densification and mechanical properties of silicon nitride ceramics were inverstigated.The results show that the introduction of tungsten carbide effectively reduces the activation energy of β phase precipitation and growth, which promotes the phase transformation of silicon nitride ceramic , and the densification of sintered samples. Tungsten carbide can dissolve into the matrix lattice partly.With the increase of the amount of tungsten carbide, the flexural strength of sintered samples increased from 735.2MPa to 1091.2MPa, which increased by 48.4%.

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[Liu Jian, Li Zhijian, Luo Xudong, Xie Zhipeng. Effect of Tungsten Carbide on Densification and Mechanical Properties of Silicon Nitride Ceramics by Spark Plasma Sintering[J]. Rare Metal Materials and Engineering,2018,47(S1):241~244.]
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History
  • Received:June 23,2017
  • Revised:March 01,2018
  • Adopted:March 05,2018
  • Online: October 22,2018
  • Published: